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Characterization of TiO2 quantum dots synthesized by hydrothermal method

机译:水热法合成TiO 2 量子点的表征

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摘要

TiO2 quantum dots were synthesized by a hydrothermal method after precipitating titanium hydroxide using Ti(SO4)2 and NaOH solutions. A simple hydrothermal apparatus was manufactured in the laboratory and operated at temperature 100℃, 130℃, and 160℃. Spherical, uniform, and non-aggregated approximately 15 nm in size TiO2 quantum dots were obtained. Properties of synthesized TiO2 quantum dots were characterized using UV/Vis/NIR spectrophotometry, XRD diffractometry, and TEM.
机译:利用Ti(SO 4 2 和NaOH溶液沉淀氢氧化钛后,通过水热法合成了TiO 2 量子点。在实验室中制造了一种简单的水热仪器,并在100℃,130℃和160℃的温度下运行。获得了球形,均匀且未聚集的约15 nm的TiO 2 量子点。利用UV / Vis / NIR分光光度法,XRD衍射和TEM对合成的TiO 2 量子点的性质进行了表征。

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