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Microwave Assisted Green Synthesis of Silver Nanoparticles Using Mulberry Leaves Extract and Silver Nitrate Solution

机译:桑叶提取物和硝酸银溶液微波辅助绿色合成纳米银

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In this work, silver nanoparticles (AgNPs) were synthesized quickly and in an eco-friendly manner using the extract of Mulberry leaves and aqueous solution of silver nitrate without any toxic chemicals (Yuet et al. Int. J. Nanomed. 2012 , 7 , 4263–4267; Krishnakuma and Adavallan. Adv. Nat. Sci. Nanosci. Nanotechnol. 2014 , 5 , 025018). The Mulberry leaves extract functions as both a stabilizing and reducing agent. The UV-Vis spectroscopy shows a peak maximum at 430 nm. The transmission electron microscopy (TEM) image illustrated of synthesized AgNPs were nearly spherical-shaped particles whose sizes range from 15 to 20 nm. The TEM image of Nano Silver solution sample synthesized by the microwave assisted method shows nearly spherical particles, with an average particle size estimated at 10 nm. The absorption UV-vis spectrum of silver nanoparticles synthesized by the microwave assisted method (AgNPsmw) shows a sharp absorption band around 415 nm. The UV-Vis spectrum of AgNPsmw after two months of storage shows negligible peak changes of silver nanoparticles.
机译:在这项工作中,使用桑叶提取物和硝酸银水溶液,不含任何有毒化学物质,以生态友好的方式快速合成了银纳米颗粒(AgNPs)(Yuet et al。Int。J. Nanomed。2012,7, 4263–4267; Krishnakuma和Adavallan。Adv。Nat。Sci。Nanosci.Nanotechnol。2014,5,025018)。桑叶提取物既起稳定剂的作用,又起还原剂的作用。紫外-可见光谱在430 nm处显示最大峰值。合成的AgNPs的透射电子显微镜(TEM)图像是接近球形的颗粒,尺寸范围为15到20 nm。通过微波辅助方法合成的纳米银溶液样品的TEM图像显示出近乎球形的颗粒,平均粒径估计为10 nm。通过微波辅助方法(AgNPsmw)合成的银纳米粒子的吸收紫外可见光谱显示在415 nm附近有一个清晰的吸收带。储存两个月后,AgNPsmw的紫外-可见光谱显示银纳米颗粒的峰变化可忽略不计。

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