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Valida??o do método de determina??o simultanea dos íons brometo e bromato por cromatografia i?nica em águas de consumo humano

机译:离子色谱法同时测定饮用水中溴离子和溴离子的方法的验证

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European Directive (98/83/CE), compulsory after 2008, states that bromate in drinking water must be controlled at levels below 10 mg L-1. Supporting implementation of the Directive, the European Comission has established project SMT4-CT96 2134, in collaboration with various european institutions, aiming at the identification of the interferents to the current analytical method (Ionic Chromatography with Conductimetric Detection - IC/CD), their removal and the automation of pre-treatment and injection steps, as well as the development of alternative methods. EPAL, responsible for the water supply to a great deal of Portuguese regions, has taken steps to meet these requirements. Although not part of such project, this work (the result of a project conducted under a protocol of collaboration between EPAL SA and FCUL - Faculty of Sciences, University of Lisbon), reports on studies of usefulness to laboratories planning to monitor bromate in ozone treated waters, in conditions different from those described in EPA 300.1. Simultaneous determination of bromide is justified by its role as bromate precursor.
机译:2008年后强制执行的欧洲指令(98/83 / CE)指出,饮用水中的溴酸盐必须控制在10 mg L-1以下。为支持该指令的实施,欧洲委员会与多家欧洲机构合作建立了SMT4-CT96 2134项目,旨在识别当前分析方法(带电导检测的离子色谱法-IC / CD)的干扰物,并去除它们。以及自动化的预处理和注射步骤,以及替代方法的开发。负责向葡萄牙大部分地区供水的EPAL已采取措施来满足这些要求。尽管不是该项目的一部分,但这项工作(根据EPAL SA和FCUL之间的合作协议进行的项目结果-里斯本大学理学院)报告了对计划监测经过臭氧处理的溴酸盐的实验室的有用性研究报告在与EPA 300.1中所述条件不同的水域中使用。同时确定溴化物作为溴酸盐前体的作用是合理的。

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