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Updating undergraduate experimental organic chemistry

机译:更新本科实验有机化学

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The present contribution describes three different modern experiments for possible adoption in undergraduate organic chemistry laboratories. These are: 1. electrocatalytic hydrogenation of benzaldehyde to benzyl alcohol; 2. identification of three volatile components, obtained from pineapple fruit, by mass spectrometry and 3. microwave mediated fast synthesis of N-(p-chlorophenyl)phthalamic acid from phthalic anhydride and p-chloroaniline under solvent-free conditions. The experiments can be executed in a short period of time, putting the undergraduate student in contact with a variety of topics in organic chemistry and several techniques of analysis, showing multidisciplinarity in organic chemistry.
机译:本文稿描述了三种不同的现代实验,这些实验可能会在本科生有机化学实验室中采用。它们是:1.苯甲醛电催化加氢为苯甲醇; 2.通过质谱法鉴定从菠萝果实中获得的三种挥发性成分,并且3.在无溶剂的条件下,由微波介导的邻苯二甲酸酐和对氯苯胺快速合成N-(对氯苯基)邻苯二甲酸。实验可以在短时间内完成,使本科生接触到有机化学的各种主题和几种分析技术,显示出有机化学的多学科性。

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