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Preparation and Characterization of Supported Photocatalytic Composite and its Decomposition and Disinfection Effect on Bacteria in Municipal Sewage WaterS

机译:负载型光催化复合材料的制备,表征及其对城市污水中细菌的分解消毒作用

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TiO_(2)/CASB was prepared by straight forward mild hydrothermal processes. As prepared photocatalytic materials were characterized by powder X-ray diffraction (XRD), Scanning Electron Microcopy (SEM), Fourier Transform Infrared spectroscopy (FTIR), Positrons Annihilation Lifetime Spectroscopy (PALS) and Inductively Coupled Plasma Mass Spectroscopy (ICP-MS) to assess their physicochemical properties. Their photocatalytic decomposition and disinfection activity of bacteria in municipal sewage water was studied. The XRD studies reveal the presence of TiO in the form of anatase phase in the supported composite. The XRD studies further suggested that well crystalline form of TiO_(2) onto calcium alumino silicate beads (CASB) supports. FTIR results revealed the presence of Ti-O-Si linkages in the TiO_(2)/CASB composite, which are responsible for its higher photocatalytic activity in the destruction of bacterial mass in the sewage water. TiO_(2) deposited CASB composite showed drastic reduction in the colony forming unit (CFU) of sewage water with UV light.
机译:TiO_(2)/ CASB通过直接温和的水热法制备。所制备的光催化材料通过粉末X射线衍射(XRD),扫描电子显微镜(SEM),傅立叶变换红外光谱(FTIR),正电子An没寿命光谱(PALS)和电感耦合等离子体质谱(ICP-MS)进行表征。评估其理化性质。研究了它们对城市污水中细菌的光催化分解和消毒活性。 XRD研究表明,负载的复合材料中存在锐钛矿相形式的TiO。 XRD研究进一步表明,TiO_(2)的良好结晶形式存在于铝硅酸钙微珠(CASB)载体上。 FTIR结果表明,在TiO_(2)/ CASB复合材料中存在Ti-O-Si键,这是由于其较高的光催化活性可以破坏污水中的细菌。 TiO_(2)沉积的CASB复合材料在紫外线作用下显示出污水菌落形成单元(CFU)的急剧减少。

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