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Analytical methods for determination of bisphenol A, 4- tert-octylphenol and 4-nonylphenol in herrings and physiological fluids of the grey seal

机译:测定青海豹鲱鱼和生理液中双酚A,4- tert -辛基酚和4-壬基酚的分析方法

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?The aim of this work was to develop the methods of determination for phenol derivatives: bisphenol A (BPA), 4-tert-octylphenol (OP) and 4-nonylphenol (NP), in the whole body of herringClupea harengusand in physiological fluids of the Baltic grey sealHalichoerus grypus grypus(blood and milk).?Methods were based on liquid chromatography coupled with a fluorescence detector (HPLC-FL).?These methods were satisfactorily validated, each showing good recovery (>80%) and precision (RSD?
机译:这项工作的目的是开发鲱鱼浑身中的豌豆和生理液中双酚A(BPA),4-叔辛基苯酚(OP)和4-壬基苯酚(NP)酚衍生物的测定方法。波罗的海豹(Halichoerus grypus grypus)(血液和牛奶)。基于液相色谱和荧光检测器(HPLC-FL)的方法。这些方法均得到令人满意的验证,每种方法均具有良好的回收率(> 80%)和精密度(RSD)。 ≤15%)。关于定量限(LOQ),鲱鱼的定量限为<2 ng?g?1,血液的定量限为<0.07 ng?cm-3,牛奶的定量限为<0.1 ng?cm?3。

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