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Hot Deformation Behavior and Microstructure Evolution of a TiB w /Near α-Ti Composite with Fine Matrix Microstructure

机译:具有精细基体组织的TiB w /近α-Ti复合材料的热变形行为和组织演变

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The hot deformation behavior and microstructure evolution of a 7.5 vol.% TiB w ear α-Ti composite with fine matrix microstructure were investigated under the deformation conditions in a temperature range of 800–950 °C and strain rate range of 0.001–1 s ?1 using plane strain compression tests. The flow stress curves show different characteristics according to the various deformation conditions. At a higher strain rate (1 s ?1 ), the flow stress of the composite continuously increases until a peak value is reached. The activation energy is 410.40 kJ/mol, much lower than the activation energy of as-sintered or as-forged composites. The decreased activation energy is ascribed to the breaking of the TiB w reinforcement during the multi-directional forging and the resultant fine matrix microstructure. Refined reinforcement and refined matrix microstructure significantly improve the hot deformation ability of the composite. The deformation conditions determine the morphology and fraction of α and β phases. At 800–900 °C and 0.01 s ?1 the matrix α grains are much refined due to the continuous dynamic recrystallization (CDRX). The processing map is constructed based on the hot deformation behavior and microstructure evolution. The optimal hot processing window is determined to be 800–950 °C/0.001–0.01 s ?1 , which lead to CDRX of primary α grains or dynamic recovery (DRV) and dynamic recrystallization (DRX) of β phase.
机译:研究了在800-950°C的温度范围和0.001-1 s的应变率范围内的变形条件下,具有7.5%体积百分比的TiB w /近α-Ti复合材料的热变形行为和微观结构演变,该复合材料具有精细的基体组织。 1采用平面应变压缩试验。流动应力曲线根据各种变形条件显示出不同的特性。在较高的应变速率(1 s?1)下,复合材料的流动应力持续增加,直到达到峰值。活化能为410.40 kJ / mol,远低于烧结或锻造复合材料的活化能。活化能的降低归因于多方向锻造过程中TiB w增强材料的断裂以及所形成的精细基体微观结构。细化的增强材料和细化的基体微观结构显着提高了复合材料的热变形能力。变形条件决定了α相和β相的形态和分数。在800–900°C和0.01 s?1的条件下,由于连续动态重结晶(CDRX),基体α晶粒得以细化。根据热变形行为和微观组织演变构造加工图。最佳热处理窗口确定为800-950°C / 0.001-0.01 s?1,这会导致初级α晶粒的CDRX或β相的动态恢复(DRV)和动态重结晶(DRX)。

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