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Synthesis of CuO/Co3O4Coaxial Heterostructures for Efficient and Recycling Photodegradation

机译:高效和循环光降解CuO / Co3O4同轴异质结构的合成

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The highly efficient CuO/Co3O4composite photocatalyst with different morphologies has been synthesized directly on Cu wire mesh by controlling the composition of cobalt-containing solid precursors via a simple hydrothermal method. The structure morphology and composition of the composite photocatalyst have been characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), and UV-visible diffuse reflectance spectra. The photocatalytic result shows that the CuO/Co3O4coaxial heterostructure is easy to recycle and exhibit enhanced photodegradation activity for methylene blue compared to single CuO nanorod arrays under full spectrum solar light irradiation. The enhanced photocatalytic efficiency of the composite could be ascribed to the synergistic effect of CuO and Co3O4. This study provides a general and effective method in the fabrication of 1D composition NRs with sound heterojunctions that show enhancement of photocatalytic performance and facility of recycling.
机译:通过简单的水热法控制含钴固体前驱体的组成,可以直接在铜丝网上直接合成具有不同形态的高效CuO / Co3O4复合光催化剂。通过扫描电子显微镜(SEM),透射电子显微镜(TEM),X射线衍射(XRD),X射线光电子能谱(XPS)和紫外可见漫反射来表征复合光催化剂的结构形态和组成。光谱。光催化结果表明,与单一CuO纳米棒阵列在全光谱太阳光照射下相比,CuO / Co3O4同轴异质结构易于回收,并且对亚甲基蓝表现出增强的光降解活性。复合材料光催化效率的提高归因于CuO和Co3O4的协同作用。这项研究提供了一种通用且有效的方法,用于制造具有良好异质结的一维合成NR,这些NR显示出光催化性能的提高和再循环的便利性。

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