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Catalytic reduction of methylene blue and Congo red dyes using green synthesized gold nanoparticles capped by salmalia malabarica gum

机译:使用由萨拉马里亚马拉巴利卡胶封端的绿色合成金纳米颗粒催化还原亚甲基蓝和刚果红染料

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摘要

Stable gold nanoparticles (AuNPs) were synthesized using salmalia malabarica gum as both reducing and capping agent. It is a simple and eco-friendly green synthesis. The successful formation of AuNPs was confirmed by UV–visible spectroscopy (UV–Vis), Fourier transform infrared spectroscopy (FTIR), X-ray powder diffraction and transmission electron microscopy (TEM). The synthesized AuNPs were characterized by a peak at 520–535?nm in the UV–Vis spectrum. The X-ray diffraction studies indicated that the resulting AuNPs were highly crystalline with face-centred cubic geometry. TEM studies showed that the average particle size of the synthesized AuNPs was 12?±?2?nm. FTIR analysis revealed that –OH groups present in the gum matrix might be responsible for the reduction of Au+3 into AuNPs. The synthesized AuNPs exhibited good catalytic properties in the reduction of methylene blue and Congo red.
机译:稳定的金纳米颗粒(AuNPs)是用莎草(Salmalia malabarica)胶作为还原剂和封端剂合成的。这是一种简单且环保的绿色合成方法。紫外可见光谱(UV-Vis),傅立叶变换红外光谱(FTIR),X射线粉末衍射和透射电子显微镜(TEM)证实了AuNP的成功形成。合成的AuNPs在UV-Vis光谱中的一个峰值为520-535?nm。 X射线衍射研究表明,生成的AuNPs是高度结晶的,具有面心立方几何形状。 TEM研究表明,合成的AuNP的平均粒径为12±±2±2nm。 FTIR分析表明,胶基体中存在的–OH基团可能是将Au + 3还原为AuNPs的原因。合成的AuNPs在还原亚甲基蓝和刚果红方面表现出良好的催化性能。

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