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Synthesis and Characterization of Titania Nanotube-Carbon Nanotube Composite for Degradation of Phenol

机译:降解苯酚的二氧化钛纳米管-碳纳米管复合材料的合成与表征

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Titania nanotube (TNT)-carbon nanotube (CNT) composite had been successfully synthesized using simple mixing under acidic conditions and ultrasonic treatment. The samples were further characterized via field emission scanning electron microscopy (FESEM), X–ray diffraction (XRD), diffuse re?ectance UV-vis spectroscopy, and Brunauer-Emmett-Teller (BET) analysis. The TNT–CNT composite’s ability to degrade phenol, a model of industrial waste, was tested. The effects of CNT composition and calcination temperature on the phenol degradation performance of TNT-CNT composite were investigated. The results show that the TNT-CNT composite exhibits higher photocatalytic activity than TNT or CNT alone. The crystallinity of the catalyst is not the only parameter affecting the photocatalytic activity. Rather, the specific surface area, bandgap, and morphology of the catalyst must also be considered.
机译:通过在酸性条件下简单混合和超声处理成功地合成了二氧化钛纳米管(TNT)-碳纳米管(CNT)复合材料。通过场发射扫描电子显微镜(FESEM),X射线衍射(XRD),漫反射紫外可见光谱和Brunauer-Emmett-Teller(BET)分析进一步表征了样品。测试了TNT-CNT复合材料降解苯酚(一种工业废物模型)的能力。研究了碳纳米管组成和煅烧温度对TNT-CNT复合材料苯酚降解性能的影响。结果表明,TNT-CNT复合材料比单独的TNT或CNT具有更高的光催化活性。催化剂的结晶度不是影响光催化活性的唯一参数。而是,还必须考虑催化剂的比表面积,带隙和形态。

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