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Effect of Annealing Temperature on Microstructure and Mechanical Properties of Ultrafine Grained Brass Produced by Equal Channel Angular Pressing

机译:退火温度对等径角挤压超细晶粒黄铜组织和力学性能的影响

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The present study investigated the mechanical properties and microstructure of ultrafine grained (UFG) brass processed by four passes of equal channel angular pressing (ECAP) and annealed at elevated temperatures. The mechanical properties of all samples were assessed using tensile and micro-hardness tests. Microstructure analysis was performed using optical microscopy (OM) and scanning electron microscopy (SEM). Ultimate tensile strengths (UTS) and yield strengths (YS) of 878 and 804 MPa, respectively, ductility of 15%, and hardness of 248 HV were obtained for samples processed by four passes of ECAP with equivalent true strain of 4.20. Annealing at 300°C caused UTS and YS to decrease significantly, to 510 and 408 MPa, respectively, ductility to increase to 28%, and hardness to decrease to 165 HV. Fractography analysis of un-annealed samples after four ECAP passes showed small brittle fractures with shallow dimpling. Ductile failures were found on annealed samples. After four ECAP passes, the microstructure of un-annealed samples was UFG and dominated by lamellar grain with shear band. In contrast, after annealing, the microstructure changed due to recrystallization, showing nucleation and grain growth.
机译:本研究研究了四道等通道角向压制(ECAP)并在高温下退火的超细晶粒(UFG)黄铜的机械性能和显微组织。使用拉伸和显微硬度测试评估所有样品的机械性能。使用光学显微镜(OM)和扫描电子显微镜(SEM)进行微观结构分析。对于通过ECAP四次通过的等效真实应变为4.20的样品,其极限抗拉强度(UTS)和屈服强度(YS)分别为878和804 MPa,延展性为15%,硬度为248 HV。在300°C的退火温度下,UTS和YS分别显着降低至510和408 MPa,延展性提高至28%,硬度降低至165 HV。四次ECAP通过后未退火样品的分形分析表明,脆性断裂较小,凹陷浅。在退火的样品上发现延性失效。经过四次ECAP处理后,未退火样品的微观结构为UFG,并以带剪切带的层状晶粒为主。相反,退火后,显微组织由于重结晶而改变,显示出成核和晶粒长大。

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