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Investigation on the structural, morphological and photochemical properties of spin-coated TiO2 and ZnO thin films prepared by sol-gel method

机译:溶胶-凝胶法制备旋涂TiO2和ZnO薄膜的结构,形貌和光化学性质的研究

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In this study, TiO2 and ZnO nanofilms were prepared by sol-gel spin-coating method. Nanofilms were characterized by X-ray Diffraction (XRD), Energy Dispersive Analysis of????? X-ray (EDX), Scanning Electron Microscopy (SEM) and Field Emission Scanning Electron Microscopy (FE-ESM). Structural and morphological properties of nanofilms were investigated. The average crystalline size of TiO2 and ZnO nanoparticles which were obtained from the ignition of sols were obtained 80 and 50 nm, respectively. The morphological properties of nanofilms showed that the TiO2/ZnO nanocomposite film was strongly related to the steps of coating. Also, photocatalytic degradation of methylene blue on the surface of these nanofilms under UV light irradiation was studied and results were compared to each other.
机译:本研究采用溶胶-凝胶旋涂法制备了TiO2和ZnO纳米薄膜。纳米膜的特征在于X射线衍射(XRD),能量分布分析。 X射线(EDX),扫描电子显微镜(SEM)和场发射扫描电子显微镜(FE-ESM)。研究了纳米膜的结构和形态特性。通过点燃溶胶获得的TiO2和ZnO纳米颗粒的平均晶体尺寸分别为80 nm和50 nm。纳米薄膜的形貌特性表明,TiO2 / ZnO纳米复合薄膜与涂覆步骤密切相关。另外,研究了在紫外线照射下这些纳米膜表面上亚甲基蓝的光催化降解,并将结果进行了比较。

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