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Synthesis and Characterization of Ag Nanoparticles Addition on BPSCCO Superconducting Thin Films

机译:BPSCCO超导薄膜上添加银纳米粒子的合成与表征

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The growth of epitaxial Ag nanoparticles doped (Bi, Pb)-2223 thin films on Si (111) substrates by pulsed laser deposition (PLD) and post-deposition oxygen annealing have been achieved. The phase identification and gross structural characteristics of synthesized films explored through X-ray diffractometer reveal that all the samples crystallize in orthorhombic structure. DC electrical resistivity measurements were done by the standard four-probe method and the results showed improvement in Tc by increasing Ag nanoparticles to 1.0 wt% which had a maximum enhancement in Tc for all investigated films. The surface morphology investigated through scanning electron microscope (SEM) and atomic force microscopy (AFM) results showed that an increase in Tc with the appropriate Ag nanoparticles addition in the samples is associated with the enhancement of Bi (Pb)-2223 phase formation.
机译:通过脉冲激光沉积(PLD)和沉积后氧退火,实现了在Si(111)衬底上外延掺杂Ag纳米粒子(Bi,Pb)-2223薄膜的生长。通过X射线衍射仪对合成膜的相鉴定和总体结构特征进行了揭示,所有样品均以正交晶结构结晶。通过标准的四探针法进行直流电阻率测量,结果表明,通过将Ag纳米颗粒增加到1.0 wt%,Tc有所改善,这对所有研究的薄膜而言Tc都有最大的提高。通过扫描电子显微镜(SEM)和原子力显微镜(AFM)研究的表面形貌表明,在样品中添加适当的Ag纳米颗粒后,Tc的增加与Bi(Pb)-2223相形成的增强有关。

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