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首页> 外文期刊>International Journal of Scientific & Technology Research >Polyetherimide (PEI) / Silicone Rubber Composite Reinforced With Nanosilica Particles
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Polyetherimide (PEI) / Silicone Rubber Composite Reinforced With Nanosilica Particles

机译:纳米二氧化硅颗粒增强的聚醚酰亚胺(PEI)/硅橡胶复合材料

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摘要

The present investigation is aimed to prepare polyetherimide (PEI)/silicone rubber nanocomposites reinforced with various amounts of loading (phr) of modified nanosilica using melt mixing process with the help of co-rotating twin screw extruder. Microstructures of the developed nanocomposites have been studied by XRD and SEM. Thermal properties of the developed nanocomposites have been analyzed by TGA. Developed nanocomposites have shown remarkable improvement in mechanical, thermal and morphological properties due to better interfacial adhesion between nanosilica and polymer matrix at 3 phr loading of nanofillers. The addition of nanosilica in polymer matrix has enhanced the thermal stability appreciably at 3 phr loading. This might be attributed to excellent interfacial adhesion and interaction between the nanosilica particles and polymer matrix. SEM micrographs reveal that the entire surface of developed nanocomposites is smooth and has no voids and cavities. It is also evident from SEM images that there is excellent dispersion of nanosilica throughout the entire polymer matrix. Mechanical properties results demonstrate that there is significant in modulus, strength, hardness, impact etc. due to its uniform and homogeneous dispersion of nanosilica in polymer matrix.
机译:本研究旨在通过同向旋转双螺杆挤出机的熔融混合工艺来制备以各种负载量(phr)的改性纳米二氧化硅增强的聚醚酰亚胺(PEI)/硅橡胶纳米复合材料。 XRD和SEM研究了已开发的纳米复合材料的微观结构。通过TGA分析了所开发的纳米复合材料的热性质。由于在3份装填量的纳米填料中,纳米二氧化硅和聚合物基质之间的界面粘合性更好,因此已开发的纳米复合材料在机械,热学和形态学性能方面已取得显着改善。在聚合物基质中添加纳米二氧化硅可显着提高3 phr负载下的热稳定性。这可能归因于纳米二氧化硅颗粒与聚合物基质之间出色的界面粘合性和相互作用。 SEM显微照片显示,已开发的纳米复合材料的整个表面光滑,没有空隙和孔洞。从SEM图像还可以看出,纳米二氧化硅在整个聚合物基质中具有优异的分散性。力学性能结果表明,由于纳米二氧化硅在聚合物基质中的均匀而均匀的分散,因此具有显着的模量,强度,硬度,冲击性等。

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