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α-MoO3thin films prepared by spray pyrolysis

机译:喷雾热解法制备α-MoO3薄膜

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MoO3 thin films have been deposited on clean glass slides using the spray pyrolysis technique. The samples were grown with different thicknesses by spraying on common glass substrates a solution of (ammoniummolybdatetetrahydrate) ((NH3)6Mo7O244H2O). The samples were characterized by X-ray diffraction (XRD), infrared spectroscopy, scanning electron microscopy (SEM) and electrically through electrical resistivity measurements as a function of temperature. It was found that samples present crystalline structure associated with the alpha phase of MoO3grown with preferential direction of growth along the planes (0k0). As result of increasing the volume of precursor solution sample surface becomes porous. The change in electrical resistance of MoO3 films by exposure to carbon monoxide (CO) at room temperature, makes the films obtained by this technique could be promising in its use in gas sensing devices at room temperature.
机译:MoO3薄膜已使用喷雾热解技术沉积在干净的载玻片上。通过在普通玻璃基板上喷涂四水合钼酸铵((NH3)6Mo7O244H2O)溶液,使样品生长不同的厚度。通过X射线衍射(XRD),红外光谱,扫描电子显微镜(SEM)以及通过电阻率的电学测量来表征样品的温度。发现样品呈现出与MoO3的α相相关的晶体结构,并沿平面(0k0)优先生长。由于增加前体溶液的体积,样品表面变得多孔。通过在室温下暴露于一氧化碳(CO)来改变MoO3薄膜的电阻,使得通过这种技术获得的薄膜在室温下在气体传感设备中的应用前景广阔。

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