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SYNTHESIS OF ALUMINIUM BORATE WHISKERS THROUGH WET MOLTEN SALT METHOD

机译:湿法熔融盐法合成硼酸铝晶须

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Aluminium borate (Al?B?O?) whiskers were successfully synthesized by the wet molten salt method at 800 oC through control the aluminum/boron atomic ratio and synthesis temperature. The as-received Al?B?O? whiskers were characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD) and thermal analysis. A solution-liquid-solid (SLS) mechanism was proposed for the growth mechanism of the whiskers on the basis of the experimental phenomena and the TG-DSC data of the mixed raw materials.
机译:通过控制铝/硼原子比和合成温度,通过湿式熔融盐法在800 oC上成功合成了硼酸铝(Al 2 B 2 O 3)晶须。 Al?B?O?晶须通过扫描电子显微镜(SEM),X射线衍射(XRD)和热分析进行表征。根据实验现象和混合原料的TG-DSC数据,提出了晶须生长机理为固液固(SLS)机理。

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