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Synthesis and Characterization of Iron (III) Oxide Nanomaterials for Photocatalytic Degradation of Congo Red

机译:氧化铁(III)纳米材料的光催化降解刚果红的表征

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This paper reports the synthesis and characterization nano-sized Iron (III) oxide for photochemical degradation of reactive Congo red (CR). The Fe 2 O 3 nanoparticles were prepared by simple aqueous combustion synthesis method using Fe(NO 3 ) 3 .9H 2 O as an oxidant and N 2 H 4 CO as fuel at 1:1 ratio. The synthesized photocatalysts were characterized by XRD, SEM, FTIR and Uv-vis Spectroscopy. The synthesized samples were tested as photocatalysts for the decomposition of Congo red dye under UV irradiation. The impact of crystal size, loading catalyst and irradiation time on the rate of decomposition of Congo red dye was investigated. The experimental results show that CR degradation increased with increasing of crystal size, time and amount of loaded catalyst.
机译:本文报道了用于反应性刚果红(CR)光化学降解的纳米级氧化铁(III)的合成与表征。通过简单的水燃烧合成法,以Fe(NO 3)3 .9H 2 O为氧化剂,N 2 H 4 CO为燃料,以1:1的比例制备了Fe 2 O 3纳米粒子。通过XRD,SEM,FTIR和紫外可见光谱对合成的光催化剂进行了表征。测试合成的样品作为光催化剂,以在紫外线照射下分解刚果红染料。研究了晶体大小,负载催化剂和辐照时间对刚果红染料分解速率的影响。实验结果表明,CR的降解随着晶体尺寸,时间和催化剂用量的增加而增加。

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