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Uso de quitina como um composto auxiliar na prepara??o de ZSM-5 mesoestruturada

机译:甲壳素作为辅助化合物在制备介孔结构ZSM-5中的用途

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In this work, mesostructured ZSM-5 zeolite was prepared using chitin as a new template to produce mesoporosity . Different amounts of chitin were used for the synthesis of ZSM-5 in order to verify its influence on the formation of mesopores. All samples were prepared by conventional hydrothermal process. For comparison purposes, ZSM-5 zeolite has also been synthesized without a presence of chitin. The samples were characterized by X-ray diffraction, scanning electron microscopy and N 2 adsorption techniques. Experimental results showed that the mesopores volume of the obtained samples increased with increasing amount of chitin in the reaction mixture. Therefore, chitin showed to be a promising template for obtaining the ZSM-5 with mesoporous property.
机译:在这项工作中,使用甲壳质作为产生介孔性的新模板制备了介孔结构的ZSM-5沸石。为了验证ZSM-5对中孔形成的影响,使用了不同量的几丁质用于ZSM-5的合成。所有样品均通过常规水热法制备。为了比较,还已经在没有甲壳质的情况下合成了ZSM-5沸石。通过X射线衍射,扫描电子显微镜和N 2吸附技术对样品进行表征。实验结果表明,所得样品的中孔体积随着反应混合物中甲壳素含量的增加而增加。因此,几丁质是获得具有介孔性质的ZSM-5的有希望的模板。

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