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Measurement of Volumetric Mass Transfer Coefficient in Bubble Columns

机译:鼓泡塔中体积传质系数的测量

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摘要

The paper presents a brief overview of experiments on volumetric mass transfer coefficient in bubble columns. The available experimental data published are often incomparable due to the different type of gas distributor and different operating conditions used by various authors. Moreover, the value of the coefficient obtained experimentally is very sensitive to the particular method and to the physical models used in its evaluation. It follows that the Dynamic Pressure Method (DPM) is able to provide physically correct values not only in lab-scale contactors but also in pilot-scale reactors. However, the method was not correctly proven in bubble columns. In present experiments, DPM was employed in a laboratory-scale bubble column with a coalescent phase and tested in the pure heterogeneous flow regime. The method was successfully validated by the measurements under two different conditions relevant to the mass transfer. First, the ideal pressure step was compared with the non-ideal pressure step. Second, the pure oxygen absorption was compared with the simultaneous oxygen-and-nitrogen absorption. The obtained results proved that DPM is suitable for measuring the mass transport in bubble columns and to provide reliable data of volumetric mass transfer coefficient.
机译:本文简要介绍了气泡塔中体积传质系数的实验。由于各种类型的气体分配器和不同的操作条件,出版的可用实验数据通常无法比拟。而且,通过实验获得的系数值对特定方法及其评估中使用的物理模型非常敏感。因此,动态压力法(DPM)不仅可以在实验室规模的接触器中而且在中试规模的反应堆中也可以提供物理上正确的值。但是,该方法未在鼓泡塔中正确验证。在当前的实验中,DPM被用于具有聚结相的实验室规模的鼓泡塔中,并在纯的非均相流动状态下进行了测试。通过在与传质相关的两个不同条件下的测量成功验证了该方法。首先,将理想压力步骤与非理想压力步骤进行了比较。其次,将纯氧吸收与同时吸收氧和氮进行了比较。所得结果证明,DPM适用于测量气泡塔中的传质,并提供可靠的体积传质系数数据。

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