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COMPLEXING AGENT EFFECT ON THE PROPERTIES OF IRON SULPHIDE THIN FILMS

机译:络合剂对硫化铁薄膜性能的影响

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Thin films of iron sulphide were prepared by chemical bath deposition technique in aqueous solutions. The influence of complexing agent for the formation of thin films was determined. The structure, morphology and optical properties of thin films of iron sulphide grown on microscope glass slide were investigated by X-ray diffraction, scanning electron microscopy and UV-Vis spectrophotometer. The films deposited using 0.1 M of sodium tartrate indicated the highest number of FeS peaks and covered substrate surface completely based on X-ray diffraction data and scanning electron microscopy results, respectively. However, when the concentration of sodium tartrate was increased to 0.2 M and above, the number of FeS peaks decreased and the films showed incomplete coverage of material over the surface of the substrate with inhomogeneous grain size.
机译:通过化学浴沉积技术在水溶液中制备硫化铁薄膜。确定了络合剂对薄膜形成的影响。通过X射线衍射,扫描电子显微镜和紫外可见分光光度计研究了在显微镜载玻片上生长的硫化铁薄膜的结构,形态和光学性质。根据X射线衍射数据和扫描电子显微镜结果,分别使用0.1 M的酒石酸钠沉积的薄膜显示出最高的FeS峰数和完全覆盖的基材表面。然而,当酒石酸钠的浓度增加到0.2 M或更高时,FeS峰的数量减少,并且膜显示出材料在基板表面上的材料覆盖不完全,并且晶粒尺寸不均匀。

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