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Preparation and investigation of Ala€“4 wt% B4C nanocomposite powders using mechanical milling

机译:机械研磨制备Ala€4 wt%B4C纳米复合粉体

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Boron carbide nanoparticles were produced using commercially available boron carbide powder (0.8 e???m).Mechanical milling was used to synthesize Al nanostructured powder in a planetary ball-mill under argon atmosphere up to 20 h. The same process was applied for Ala€“4 wt% B4C nanocomposite powders to explore the role of nanosize reinforcements on mechanical milling stages. Scanning electron microscopy (SEM) analysis as well as apparent density measurements were used to optimize the milling time needed for completion of the mechanical milling process. The results show that the addition of boron carbide particles accelerate the milling process, leading to a faster work hardening rate and fracture of aluminum matrix. FE-SEM images show that distribution of boron carbide particles in aluminum matrix reaches a full homogeneity when steady state takes place. The better distribution of reinforcement throughout the matrix would increase hardness of the powder. To study the compressibility of milled powder, modified heckel equation was used to consider the pressure effect on yield strength as well as reinforcing role of B4C particles. For better distribution of reinforcement throughout the matrix, e?‘?, modified heckel equation was used to consider the pressure effect on yield strength as well as reinforcing role of B4C particles.
机译:使用市售的碳化硼粉末(0.8 e·m)生产碳化硼纳米颗粒。在行星式球磨机中,在氩气气氛下长达20小时,使用机械研磨合成Al纳米结构粉末。将相同的工艺应用于Ala?4 wt%B 4 C纳米复合粉末,以探索纳米尺寸增强材料在机械研磨阶段的作用。使用扫描电子显微镜(SEM)分析以及表观密度测量来优化完成机械研磨过程所需的研磨时间。结果表明,碳化硼颗粒的加入加速了铣削过程,从而导致更快的加工硬化速率和铝基体的断裂。 FE-SEM图像表明,当稳态发生时,碳化硼颗粒在铝基体中的分布达到完全均匀。增强剂在整个基质中的更好分布将增加粉末的硬度。为了研究磨粉的可压缩性,使用修正的heckel方程来考虑压力对屈服强度的影响以及B 4 C颗粒的增强作用。为了使增强物更好地分布在整个基体中,使用改进的heckel方程来考虑压力对屈服强度的影响以及B 4 C颗粒的增强作用。

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