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Influence of nanometric silicon carbide on phenolic resin composites properties

机译:纳米碳化硅对酚醛树脂复合材料性能的影响

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This paper presents a preliminary study on obtaining and characterization of phenolic resin-based composites modified with nanometric silicon carbide. The nanocomposites were prepared by incorporating nanometric silicon carbide (nSiC) into phenolic resin at 0.5, 1 and 2 wt% contents using ultrasonication to ensure uniform dispersion of the nanopowder, followed by heat curing of the phenolic-based materials at controlled temperature profile up to 120$^{circ}$C. The obtained nanocomposites were characterized by FTIR spectroscopy and scanning electron microscopy analysis and evaluated in terms of mechanical, tribological and thermal stability under load. The results highlight the positive effect of the nanometric silicon carbide addition in phenolic resin on mechanical, thermo-mechanical and tribological performance, improving their strength, stiffness and abrasive properties. The best results were obtained for 1 wt% nSiC, proving that this value is the optimum nanometric silicon carbide content. The results indicate that these materials could be effectively used to obtain ablative or carbona€“carbon composites in future studies.
机译:本文对纳米碳化硅改性酚醛树脂基复合材料的制备与表征进行了初步研究。纳米复合材料的制备方法是:使用超声波将纳米碳化硅(nSiC)掺入酚醛树脂中,含量为0.5%,1%和2%(重量),以确保纳米粉体均匀分散,然后在可控温度范围内将酚醛类材料加热固化至120 $ ^ {circ} $ C。通过FTIR光谱和扫描电子显微镜分析对获得的纳米复合材料进行表征,并根据载荷下的机械,摩擦学和热稳定性对其进行评估。结果突出了在酚醛树脂中添加纳米碳化硅对机械,热机械和摩擦学性能的积极影响,从而改善了它们的强度,刚度和研磨性能。对于1 wt%的nSiC,可获得最佳结果,证明该值是最佳的纳米碳化硅含量。结果表明,这些材料可以在未来的研究中有效地用于获得烧蚀或碳素复合材料。

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