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Translucency, flexural strength, fracture toughness, fracture load of 3-unit FDPs, Martens hardness parameter and grain size of 3Y-TZP materials

机译:半透明,弯曲强度,断裂韧性,3单元FDP的断裂载荷,Martens硬度参数和3Y-TZP材料的粒度

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Objective. This investigation tested pre-shaded 3Y-TZP materials on optical, mechanical and structural properties and calculated correlations between these properties.Methods. Seven A2-shaded 3Y-TZP zirconia materials were investigated on translucency (T) via UV-vis-spectrophotometer, fracture load of 3-unit FDPs (FL), biaxial flexural strength (FS), Chevron-Notch Beam (CNB), fracture toughness (KO and Martens parameter (hardness: HM and indentation modulus: E-IT). FL, FS and K-IC were measured in a universal testing machine. The grain size was evaluated by scanning electron microscopy (SEM). Data was analyzed using one-way ANOVA followed by post hoc Scheffe, Kruskal-Wallis-, Mann-Whitney-U-and Pearson-test (p 0.05).Results. For translucency, negative correlations were found with results of facture load (R = -0.444, p 0.001) and K-IC (R = -0.503, p 0.001). While a positive correlation was found between translucency and flexural strength (R = 0.238, p = 0.019), between fracture load and E-IT (R = 0.227, p 0.029), between fracture load and K-IC (R = 0.362, p 0.001) as well as between fracture load and the grain size (R = 0.598, p = 0.007). While the grain size positively correlated with E-IT (R = 0.534, p = 0.017) as well as E-IT with HM (R = 0.720, p 0.001).Significance. Despite of being based on the same raw material, tested zirconia materials significantly differed regarding optical, mechanical (except biaxial flexural strength and Martens hardness) and structural properties. Materials with highest optical properties were those with lowest mechanical properties (CER, COP). (C) 2020 The Academy of Dental Materials. Published by Elsevier Inc. All rights reserved.
机译:客观的。该研究在光学,机械和结构性质上测试了预阴影的3Y-TZP材料,并在这些属性之间计算出相关的相关性。通过UV-Vis分光光度计,3单元FDPS(FL),双轴弯曲强度(FS),骨折 - 凹凸束(CNB),裂缝,对半透明(T)进行七A2阴影3Y-TZP氧化锆材料。韧性(KO和Martens参数(硬度:HM和缩进模量:E-it)。在通用试验机中测量FL,FS和K-IC。通过扫描电子显微镜(SEM)评估晶粒尺寸。分析数据使用单向ANOVA,然后是HOC Scheffe,Kruskal-Wallis-,Mann-Whitney-u和Pearson-Test(P <0.05)。对于半透明,有条件负荷结果发现负相关(R = - 0.444,P <0.001)和K-IC(r = -0.503,p <0.001)。在裂缝载荷和e-it之间的半透明和弯曲强度(r = 0.238,p = 0.019)之间存在正相关性(r = 0.238)( r = 0.227,p <0.029),裂缝载荷和k-ic(r = 0.362,p <0.001)以及裂缝载荷和粒度(r = 0.598,p = 0.007)之间。而g雨大小与e-it呈正相关(r = 0.534,p = 0.017)以及用hm的e-it(r = 0.720,p <0.001)。重要性。尽管基于相同的原料,但测试的氧化锆材料关于光学,机械(除副弯曲强度和Martens硬度除外)和结构性质显着不同。具有最高光学性质的材料是具有最低机械性能(CER,COP)的材料。 (c)2020牙科材料学院。由elsevier Inc.出版的所有权利保留。

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