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Preparation and Characterization of Fe/Al_2O_3 Nanocomposites

机译:Fe / Al_2O_3纳米复合材料的制备与表征

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Fe_2O_3/Al_2O_3 nanocomposites prepared by using the sol-gel technique were reduced in H_2 atmosphere at different temperatures, and the corresponding Fe/Al_2O_3 nanocomposites were obtained after the reduction of Fe_2O_3/Al_2O_3 nanocomposites at 1173 K. The structures and properties of the specimens were studied by X-ray diffraction( XRD), Moessbauer spectroscopy( MS) , and vibrating sample magnetometry( VSM). The results show that the reduction temperature has a significant influence on the structure, the grain size, and the magnetic properties of the specimens.
机译:溶胶-凝胶法制备的Fe_2O_3 / Al_2O_3纳米复合材料在不同温度下在H_2气氛中还原,在1173 K下还原Fe_2O_3 / Al_2O_3纳米复合材料得到相应的Fe / Al_2O_3纳米复合材料。通过X射线衍射(XRD),莫斯鲍尔光谱(MS)和振动样品磁力法(VSM)进行了研究。结果表明,还原温度对试样的结构,晶粒尺寸和磁性能有重要影响。

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