Monitoring the stepwise assembly of a 3-D framework from a supramolecular lanthanoid synthon by in situ infrared spectroscopy

Philip C. Andrews; William J. Gee; Peter C. Junk; Harald Krautscheid; Jonathan G. MacLellan

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Monitoring the stepwise assembly of a 3-D framework from a supramolecular lanthanoid synthon by in situ infrared spectroscopy

机译：通过原位红外光谱监测超分子镧系合成子的3-D骨架的逐步组装

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Construction of a 3-D supramolecular network from [Ln(cpb)_3(H_2O)_2] (Ln = Nd, Tb; Hcpb = l-(4-cyanophenyl)-1,3-butanedione) by sequential displacement of a coordinated water by DMF, dimerisation by reciprocal hydrogen bonding in solution and π-π stacking and interdigitation of nitriles has been monitored by in situ fourier transform infrared spectroscopy.

机译：通过依次置换配位水，从[Ln（cpb）_3（H_2O）_2]（Ln = Nd，Tb; Hcpb = 1-（4-氰基苯基）-1,3-丁二酮）构建3-D超分子网络通过DMF，已经通过原位傅立叶变换红外光谱法监测了溶液中氢相互键结的二聚作用以及π-π堆积和腈的相互指配。

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《Chemical Communications》 |2010年第32期|P.5948-5950|共3页
作者
Philip C. Andrews; William J. Gee; Peter C. Junk; Harald Krautscheid; Jonathan G. MacLellan;
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School of Chemistry, Monash University, Clayton, Melbourne, Vic 3800, Australia;

School of Chemistry, Monash University, Clayton, Melbourne, Vic 3800, Australia;

School of Chemistry, Monash University, Clayton, Melbourne, Vic 3800, Australia;

Institut fur Anorganische Chemie, Universitdt Leipzig, 04103 Leipzig, Germany;

School of Chemistry, Monash University, Clayton, Melbourne, Vic 3800, Australia;

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Monitoring the stepwise assembly of a 3-D framework from a supramolecular lanthanoid synthon by in situ infrared spectroscopy

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