Synthesis of lithium corrole and its use as a reagent for the preparation of cyclopentadienyl zirconium and titanium corrole complexes

Heather L. Buckley; Wayne A. Chomitz; Beata Koszarna; Mariusz Tasior; Daniel T. Gryko; Penelope J. Brothers; John Arnold

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Synthesis of lithium corrole and its use as a reagent for the preparation of cyclopentadienyl zirconium and titanium corrole complexes

机译：锂甲氧基化物的合成及其在制备环戊二烯基锆钛杂化物中的应用

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The lithium corrole complex (Mes_2(p-OMePh)corrole)Li_3· 6THF (1·6THF), prepared via deprotonation of the free-base corrole with lithium amide, acts as precursor for the preparation of cyclopentadienyl zirconium(Ⅳ) corrole (2) and pentamethylcyclo-pentadienyl titanium(Ⅳ) corrole (3).

机译：通过用酰胺化锂使游离碱甲酸酯去质子化而制得的锂甲酸酯络合物（Mes_2（p-OMePh）甲酸酯）Li_3·6THF（1·6THF）是制备环戊二烯锆（Ⅳ）甲酸酯的前体（2 ）和五甲基环戊二烯基钛（Ⅳ）腐蚀剂（3）。

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《Chemical Communications》 |2012年第87期|p.10766-10768|共3页
作者
Heather L. Buckley; Wayne A. Chomitz; Beata Koszarna; Mariusz Tasior; Daniel T. Gryko; Penelope J. Brothers; John Arnold;
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Department of Chemistry, University of California, Berkeley, California, 94720, USA;

Department of Chemistry, University of California, Berkeley, California, 94720, USA;

Institute for Organic Chemistry, Polish Academy of Sciences, Warsaw, Poland;

Institute for Organic Chemistry, Polish Academy of Sciences, Warsaw, Poland;

Institute for Organic Chemistry, Polish Academy of Sciences, Warsaw, Poland,Warsaw University of Technology, Faculty of Chemistry, Warsaw, Poland;

School of Chemical Sciences, University of Auckland, Auckland, New Zealand;

Department of Chemistry, University of California, Berkeley, California, 94720, USA;

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入库时间 2022-08-17 13:21:05

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机译：二（甲硅烷基）环戊二烯基钛和锆配合物的合成与反应性

Synthesis of lithium corrole and its use as a reagent for the preparation of cyclopentadienyl zirconium and titanium corrole complexes

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