Asymmetric Ti-crossed Claisen condensation: application to concise asymmetric total synthesis of alternaric acid

Ryohei Nagase; Yumiko Oguni; Satoko Ureshino; Hiroaki Mura; Tomonori Misaki; Yoo Tanabe

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Asymmetric Ti-crossed Claisen condensation: application to concise asymmetric total synthesis of alternaric acid

机译：不对称钛交联的克莱森缩合反应：在简明不对称全合成牛磺酸中的应用

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摘要

Asymmetric Ti-crossed Claisen condensation utilizing the dioxane-2,5-dione chiral template and its successful application to total synthesis of chiral alternaric acid are described.

机译：描述了利用二恶烷-2,5-二酮手性模板的不对称Ti交联的Claisen缩合及其成功应用于手性交替十八烷酸的全合成。

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《Chemical Communications》 |2013年第62期|7001-7003|共3页
作者
Ryohei Nagase; Yumiko Oguni; Satoko Ureshino; Hiroaki Mura; Tomonori Misaki; Yoo Tanabe;
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作者单位

Department of Chemistry, School of Science and Technology, Kwansei Gakuin University, 2-1 Gakuen, Sanda, Hyogo, 669-1337, Japan;

Department of Chemistry, School of Science and Technology, Kwansei Gakuin University, 2-1 Gakuen, Sanda, Hyogo, 669-1337, Japan;

Department of Chemistry, School of Science and Technology, Kwansei Gakuin University, 2-1 Gakuen, Sanda, Hyogo, 669-1337, Japan;

Department of Chemistry, School of Science and Technology, Kwansei Gakuin University, 2-1 Gakuen, Sanda, Hyogo, 669-1337, Japan;

Graduate School of Material Science, University of Hyogo, 3-2-1, Kohto, Kamigori Hyogo 678-1297, Japan;

Department of Chemistry, School of Science and Technology, Kwansei Gakuin University, 2-1 Gakuen, Sanda, Hyogo, 669-1337, Japan;

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入库时间 2022-08-17 13:18:32

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1. Construction of an asymmetric quaternary carbon via an asymmetric aza-Claisen rearrangement and its application in the total synthesis of (+)-α-cuparenone [J] . Nishii T., Miyamae F., Yoshizuka M., Tetrahedron, Asymmetry: The International Journal for Repid Publication on all Aspects of Asymmetry in Orgainc, Inorganic, Organometallic, Physical and Bio-Organic Chemistry . 2012,第10期

机译：通过不对称氮杂-克莱森重排构建不对称季碳及其在（+）-α-cuparenone的全合成中的应用
2. Asymmetric nitroallylation of arylboronic acids with nitroallyl acetates catalyzed by chiral rhodium complexes and its application in a concise total synthesis of optically pure (+)-gamma-lycorane [J] . Dong L, Xu YJ, Cun LF, Organic letters . 2005,第19期

机译：手性铑配合物催化芳基硼酸与乙酸硝基烯丙酯的不对称硝基烯丙基化反应及其在光学纯（+）-γ-二十烷的简明全合成中的应用
3. Asymmetric Total Synthesis of (-)-Azaspirene by Utilizing Ti-Claisen Condensation and Ti-Direct Aldol Reaction [J] . Sugi Mikiko, Nagase Ryohei, Misaki Tomonori, European journal of organic chemistry . 2016,第28期

机译：Ti-Claisen缩合和Ti-直接Aldol反应的不对称全合成（-）-氮杂螺碳烯
4. Synthesis of Optically Active Anti-β-Substituted γ,δ-Unsaturated Amino Acids via Asymmetric Thio-Claisen Rearrangement [C] . Zhihua Liu, Hongchang Qu, Xuyuan Gu American Peptide Symposium . 2009

机译：通过不对称硫爪重排的合成光学活性抗β-取代的γ，δ-不饱和氨基酸
5. Applications of palladium catalyzed asymmetric allylic alkylation: The synthesis of quaternary amino acids and efforts toward the total synthesis of terpestacin. [D] . Vance, Jennifer Ann. 2005

机译：钯催化的不对称烯丙基烷基化的应用：季氨基酸的合成和全合成萜品的努力。
6. Asymmetric Synthesis of Seven- Membered Carbocyclic Rings via a Sequential Oxyanionic 5-Exo Dig Cyclization/Claisen Rearrangement Process. Total Synthesis of (−)-Frondosin B [O] . Timo V. Ovaska, Jonathan A. Sullivan, Sami I. Ovaska, -1

机译：通过序贯含氧阴离子5外切挖环化/ Claisen重排过程七元碳环的不对称合成。的全合成（ - ） - Frondosin乙
7. Asymmetric Nitroallylation of Arylboronic Acids with Nitroallyl Acetates Catalyzed by Chiral Rhodium Complexes and Its Application in a Concise Total Synthesis of Optically Pure (+)-g-Lycorane [O] . -1

机译：芳基硼酸乙酸芳基硼酸的不对称硝基芳基乙酸乙酸盐，其简明地合成光学纯度（+） - G-氯烷的施用

Asymmetric Ti-crossed Claisen condensation: application to concise asymmetric total synthesis of alternaric acid

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