100% thiol-functionalized ethylene PMOs prepared by 'thiol acid-ene' chemistry

Dolores Esquivel; Otto van den Berg; Francisco J. Romero-Salguero; Filip Du Prez; Pascal Van Der Voort

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100% thiol-functionalized ethylene PMOs prepared by 'thiol acid-ene' chemistry

机译：通过“硫醇酸-烯”化学制备的100％硫醇官能化的乙烯PMO

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A novel thiol furationalized bis-silane PMO precursor was synthesized by highly efficient thiol acid-ene chemistry between the double bonds of 1,2-(E)-bis(triethoxysilyl)ethene and thioacetic acid. After aminolysis the self-assembly process of the formed SH-precursor with Pluronic P123 under acidic conditions yields the first 100% thiol-PMO material with good structural ordering.

机译：通过在1,2-（E）-双（三乙氧基甲硅烷基）乙烯的双键与硫代乙酸之间的高效硫醇酸-烯化学反应合成了一种新型的硫醇分型化的双硅烷PMO前体。氨解后，形成的SH前体与Pluronic P123在酸性条件下的自组装过程产生了具有良好结构有序性的第一个100％硫醇-PMO材料。

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《Chemical Communications》 |2013年第23期|2344-2346|共3页
作者
Dolores Esquivel; Otto van den Berg; Francisco J. Romero-Salguero; Filip Du Prez; Pascal Van Der Voort;
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作者单位

Center for Ordered Materials, Organometallics and Catalysis (COMOC), Department of Inorganic and Physical Chemistry, Ghent University, Krijgslaan 281-S3, B-9000 Ghent, Belgium;

Department of Organic Chemistry, Polymer Chemistry Research group (PCR), Ghent University, Krijgslaan 281-S4, B-9000 Ghent, Belgium;

Department of Organic Chemistry, Nanochemistry and Fine Chemistry Research Institute (IUIQFN), Faculty of Sciences, University of Cordoba, Campus de Rabanales, Marie Curie Building, Ctra. final. IV, km 396, 14071 Cordoba, Spain;

Department of Organic Chemistry, Polymer Chemistry Research group (PCR), Ghent University, Krijgslaan 281-S4, B-9000 Ghent, Belgium;

Center for Ordered Materials, Organometallics and Catalysis (COMOC), Department of Inorganic and Physical Chemistry, Ghent University, Krijgslaan 281-S3, B-9000 Ghent, Belgium;

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入库时间 2022-08-17 13:18:07

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6. Thiol-Functionalized Ethylene Periodic Mesoporous Organosilica as an Efficient Scavenger for Palladium: Confirming the Homogeneous Character of the Suzuki Reaction [O] . María I. López, Dolores Esquivel, César Jiménez-Sanchidrián, 2020

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100% thiol-functionalized ethylene PMOs prepared by 'thiol acid-ene' chemistry

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