Stereoselective synthesis of highly O-functionalized enantiopure 2,3,4trisubstituted tetrahydrofurans by tandem debenzylative cyclization of glycal derived 2,3-epoxy alcohols

Reddy LVR; Roy AD; Roy R; Shaw AK

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Stereoselective synthesis of highly O-functionalized enantiopure 2,3,4trisubstituted tetrahydrofurans by tandem debenzylative cyclization of glycal derived 2,3-epoxy alcohols

机译：糖衍生的2,3-环氧醇的串联脱苄基环化立体选择性合成高度O-官能化的对映纯2,3,4三取代四氢呋喃

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摘要

A new and highly efficient methodology for the construction of synthetically important highly O-functionalized enantiopure 2,3,4-trisubstituted tetrahydrofurans with three contiguous stereocenters is reported.

机译：报道了一种新的，高效的方法，用于构建具有三个连续的立体中心的，具有重要合成意义的高度O-官能化的对映纯2,3,4-三取代四氢呋喃。

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来源
《Chemical Communications》 |2006年第32期|p. 3444-3446|共3页
作者
Reddy LVR; Roy AD; Roy R; Shaw AK;
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作者单位

Cent Drug Res Inst, Div Med & Proc Chem, Lucknow 226001, Uttar Pradesh, India;

Cent Drug Res Inst, Div Sophisticated Analyt Instrumentat Facil, Lucknow 226001, Uttar Pradesh, India;

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原文格式 PDF
正文语种 eng
中图分类化学;
关键词
2; 3-DIDEOXY-ALPHA; BETA-UNSATURATED CARBOHYDRATE ENALS; SUBSTITUTED TETRAHYDROFURANS; DIASTEREOSELECTIVE SYNTHESIS; EPOXIDE OPENINGS; CYTOTOXIC ANHYDROPHYTOSPHINGOSINE; TETRASUBSTITUTED TETRAHYDROFURAN; STEREOCONTROLLED SYNTHESIS; ANNONACEOUS ACETOGENINS; DERIVATIVES; ROUTE;

机译：2;3-二脱氧-α-羟基苯甲醛;饱和的四氢呋喃酮;取代的四氢呋喃;非对映选择性的合成;环氧化合物的开口;细胞毒性的无糖植物鞘氨醇;四取代的四氢呋喃核苷;对映体;对映体;
入库时间 2022-08-17 13:29:57

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2. Stereoselective synthesis of 3,4-disubstituted tetrahydrofurans and 2,3,4-trisubstituted tetrahydrofurans using an intramolecular allylation strategy employing allylsilanes [J] . Peter J. Jervis, Benson M. Kariuki, Liam R. Cox Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2008,第16期

机译：使用烯丙基硅烷的分子内烯丙基化策略立体选择性合成3,4-二取代的四氢呋喃和2,3,4-三取代的四氢呋喃
3. One-Pot Synthesis of Enantiopure Spiro[3,4-dihydrobenzo[b][1,4]oxazine-2,3 '-oxindole] via Regio- and Stereoselective Tandem Ring Opening/Cyclization of Spiroaziridine Oxindoles with Bromophenols [J] . Hajra Saumen, Hazra Atanu, Abu Saleh S. K. The Journal of Organic Chemistry . 2019,第16期

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机译：高度立体化合成具有聚合物化试剂：1,1.Diboryl-L-烯烃的交叉偶联和三重醛加入（Z）-L，2,3,4-四甲基-2-丁烯
5. The regio- and stereoselective synthesis of 2,3,5-trisubstituted tetrahydrofurans via cyclization of epoxy diols and total synthesis of the proposed structure of mucoxin [D] . Narayan, Radha Sridhar 2004

机译：通过环氧二醇的环化和选择性合成粘液毒素的区域和立体选择性合成2,3,5-三取代的四氢呋喃
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机译：通过Regio和立体选择串联环开口/环化与苯磺烯醇酸丁基氧胆砂的串联环开口/环化的单壶合成苯磺酸3,4-二氢苯并B B B 1,4 B 1,4 1,4 1,4

Stereoselective synthesis of highly O-functionalized enantiopure 2,3,4trisubstituted tetrahydrofurans by tandem debenzylative cyclization of glycal derived 2,3-epoxy alcohols

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