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Effect of Microwave Heating Conditions on the Preparation of High Surface Area Activated Carbon from Waste Bamboo

机译:微波加热条件对废竹炭制备高表面积活性炭的影响

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摘要

The present study reports the effect of microwave power and microwave heating time on activated carbon adsorption ability. The waste bamboo was used to preparing high surface area activated carbon via microwave heating. The bamboo was carbonized for 2 h at 600℃ to be used as the raw material. According to the results, microwave power and microwave heating time had a significant impact on the activating effect. The optimal KOH/C ratio of 4 was identified when microwave power and microwave heating time were 700 W and 15 min, respectively. Under the optimal conditions, surface area was estimated to be 3441 m~2/g with pore volume of 2.093 ml/g and the significant proportion of activated carbon was microporous (62.3%). The results of Fourier transform infrared spectroscopy (FTIR) were illustrated that activated carbon surface had abundant functional groups. Additionally the pore structure is characterized using Scanning Electron Microscope (SEM).
机译:本研究报告了微波功率和微波加热时间对活性炭吸附能力的影响。废竹用于通过微波加热制备高表面积活性炭。将竹子在600℃碳化2 h作为原料。根据结果​​,微波功率和微波加热时间对活化效果有显着影响。当微波功率和微波加热时间分别为700 W和15分钟时,最佳KOH / C比为4。在最佳条件下,表面积估计为3441 m2 / g,孔体积为2.093 ml / g,活性炭的显着比例为微孔(62.3%)。傅里叶变换红外光谱(FTIR)的结果表明,活性炭表面具有丰富的官能团。另外,使用扫描电子显微镜(SEM)表征孔结构。

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  • 来源
    《High temperature materials and processes》 |2015年第7期|667-674|共8页
  • 作者单位

    Yunnan Provincial Key Laboratory of Intensification Metallurgy, Kunming, Yunnan 650093, China National Local Joint Laboratory of Engineering Application of Microwave Energy and Equipment Technology, Kunming, Yunnan 650093, China Key Laboratory of Unconventional Metallurgy, Ministry of Education, Kunming, Yunnan 650093, China Faculty of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093, China;

    Yunnan Provincial Key Laboratory of Intensification Metallurgy, Kunming, Yunnan 650093, China National Local Joint Laboratory of Engineering Application of Microwave Energy and Equipment Technology, Kunming, Yunnan 650093, China Key Laboratory of Unconventional Metallurgy, Ministry of Education, Kunming, Yunnan 650093, China Faculty of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093, China;

    Yunnan Provincial Key Laboratory of Intensification Metallurgy, Kunming, Yunnan 650093, China National Local Joint Laboratory of Engineering Application of Microwave Energy and Equipment Technology, Kunming, Yunnan 650093, China Key Laboratory of Unconventional Metallurgy, Ministry of Education, Kunming, Yunnan 650093, China Faculty of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093, China;

    Yunnan Provincial Key Laboratory of Intensification Metallurgy, Kunming, Yunnan 650093, China National Local Joint Laboratory of Engineering Application of Microwave Energy and Equipment Technology, Kunming, Yunnan 650093, China Key Laboratory of Unconventional Metallurgy, Ministry of Education, Kunming, Yunnan 650093, China;

    Yunnan Provincial Key Laboratory of Intensification Metallurgy, Kunming, Yunnan 650093, China National Local Joint Laboratory of Engineering Application of Microwave Energy and Equipment Technology, Kunming, Yunnan 650093, China Key Laboratory of Unconventional Metallurgy, Ministry of Education, Kunming, Yunnan 650093, China Faculty of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093, China;

    Yunnan Provincial Key Laboratory of Intensification Metallurgy, Kunming, Yunnan 650093, China National Local Joint Laboratory of Engineering Application of Microwave Energy and Equipment Technology, Kunming, Yunnan 650093, China Key Laboratory of Unconventional Metallurgy, Ministry of Education, Kunming, Yunnan 650093, China Faculty of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093, China;

    Yunnan Provincial Key Laboratory of Intensification Metallurgy, Kunming, Yunnan 650093, China National Local Joint Laboratory of Engineering Application of Microwave Energy and Equipment Technology, Kunming, Yunnan 650093, China Key Laboratory of Unconventional Metallurgy, Ministry of Education, Kunming, Yunnan 650093, China Faculty of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093, China;

    Yunnan Provincial Key Laboratory of Intensification Metallurgy, Kunming, Yunnan 650093, China National Local Joint Laboratory of Engineering Application of Microwave Energy and Equipment Technology, Kunming, Yunnan 650093, China Key Laboratory of Unconventional Metallurgy, Ministry of Education, Kunming, Yunnan 650093, China Faculty of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093, China;

  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);美国《化学文摘》(CA);
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    high surface area activated carbon; microwave heating; waste bamboo;

    机译:高表面积活性炭;微波加热;废竹;

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