首页> 外文期刊>Arabian Journal for Science and Engineering >Synthesis, Characterization and Biological Activity of Iron (III) Oxide and Titanium (Ⅳ) Oxide Nanoparticle Dispersed Polyester Resin Nanocomposites
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Synthesis, Characterization and Biological Activity of Iron (III) Oxide and Titanium (Ⅳ) Oxide Nanoparticle Dispersed Polyester Resin Nanocomposites

机译:氧化铁(III)和氧化钛(IV)纳米分散聚酯树脂纳米复合材料的合成,表征和生物活性

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摘要

In this work, dispersed nanoparticles of Fe_2O_3-and TiO_2-reinforced linear saturated polyester resin nanocomposites werefabricated. Nanosized oxides of iron (Ⅲ) and titanium (Ⅳ) and polyester resin were prepared throughout sol–gel depositionand polycondensation reactions, respectively. The incorporation of nanostructured metal oxides with polyester matrix wascharacterized. Molecular weight, structure, composition, morphology and electric property of composites were investigatedby gel permeation chromatography, Fourier transform infrared spectroscopy, X-ray diffraction, scanning electron microscopy,transmission electron microscopy and conductivity measurements. The obtained nanocomposites exhibit low crystallinity,high agglomeration and high conductivity due to the ionic cross-linking. Moreover, the biological activity of the fabricatednanocomposites was studied against selected strains of pathogenic bacteria and fungi. The biological effect of polyesternanocomposites has higher value than the free one. These nanocomposites will find potential sites in catalysis.
机译:在这项工作中,制备了Fe_2O_3-和TiO_2增强的线性饱和聚酯树脂纳米复合材料的分散纳米颗粒。在溶胶-凝胶沉积和缩聚反应中分别制备了铁(Ⅲ)和钛(Ⅳ)和聚酯树脂的纳米级氧化物。表征了纳米结构金属氧化物与聚酯基体的结合。通过凝胶渗透色谱,傅里叶变换红外光谱,X射线衍射,扫描电子显微镜,透射电子显微镜和电导率测量研究了复合材料的分子量,结构,组成,形貌和电性能。所得的纳米复合材料由于离子交联而具有低结晶度,高附聚性和高导电性。此外,研究了制备的纳米复合材料针对病原细菌和真菌的选定菌株的生物活性。聚酯纳米复合材料的生物学作用比游离的具有更高的价值。这些纳米复合材料将在催化中找到潜在的位点。

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