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Synthesis and magnetic properties of ordered barium ferrite nanowire arrays in AAO template

机译:AAO模板中有序钡铁氧体纳米线阵列的合成及磁性

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摘要

BaFe_(12)O_(19) nanowire arrays having single magnetic domain size (≤460nm) in anodic aluminum oxide (AAO) templates were prepared by sol-gel and self-propagating high-temperature synthesis techniques. The diameter of the nanowire arrays is approximately 70 nm and the length is about 2-4 μm. The specimens were characterized using X-ray diffraction, vibrating sample magnetometer, field emission scan electron microscope, atomic force microscopy and microwave vector network analyzer. The magnetic properties of BaFe_(12)O_(19) nanowire arrays embedded in AAO templates were measured by VSM with a field up to 1274 KA/m at room temperature. The results indicate that the nanowire arrays exhibit large saturation magnetization and high coercivity in the range of 6000 Oe and an obvious magnetic anisotropy with the easy magnetizing axis along the length of the nanowire arrays, probably due to the shape anisotropy and magneto-crystalline anisotropy. Finally the microwave absorption properties of the nanowires were discussed.
机译:通过溶胶凝胶和自蔓延高温合成技术制备了在阳极氧化铝(AAO)模板中具有单个磁畴尺寸(≤460nm)的BaFe_(12)O_(19)纳米线阵列。纳米线阵列的直径约为70nm,长度约为2-4μm。使用X射线衍射,振动样品磁力计,场发射扫描电子显微镜,原子力显微镜和微波矢量网络分析仪对样品进行表征。通过VSM在室温下以高达1274 KA / m的磁场测量嵌入在AAO模板中的BaFe_(12)O_(19)纳米线阵列的磁性能。结果表明,纳米线阵列在6000 Oe的范围内表现出较大的饱和磁化强度和高矫顽力,并且沿纳米线阵列的长度方向具有易于磁化轴的明显磁各向异性,这可能是由于形状各向异性和磁晶各向异性引起的。最后讨论了纳米线的微波吸收特性。

著录项

  • 来源
    《Applied Surface Science》 |2011年第21期|p.8974-8980|共7页
  • 作者单位

    Department of Applied Chemistry, Northwestern Polytechnical University, School of Science, Xi'an 710072, PR China;

    Department of Applied Chemistry, Northwestern Polytechnical University, School of Science, Xi'an 710072, PR China;

    Department of Applied Chemistry, Northwestern Polytechnical University, School of Science, Xi'an 710072, PR China;

    Department of Applied Chemistry, Northwestern Polytechnical University, School of Science, Xi'an 710072, PR China;

    Department of Applied Chemistry, Northwestern Polytechnical University, School of Science, Xi'an 710072, PR China;

    Department of Applied Chemistry, Northwestern Polytechnical University, School of Science, Xi'an 710072, PR China;

    Department of Applied Chemistry, Northwestern Polytechnical University, School of Science, Xi'an 710072, PR China;

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  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    sol-gel; BaFe_(12)O_(19); nanowire arrays; aao template; magnetic properties;

    机译:溶胶-凝胶;BaFe_(12)O_(19);纳米线阵列;aao模板;磁性;
  • 入库时间 2022-08-18 03:07:08

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