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Effect of microstructure on hydric strain in clay rock: A quantitative comparison

机译:微观结构对黏土中水力应变的影响:定量比较

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摘要

This paper presents a new method able to compare quantitatively strains and microstructure of a clay material. This method was applied to a Tournemire clay rock sample subjected to cyclic hydric loading in laboratory conditions. Local strains of a centimeter-size Tournemire clay rock sample were quantified by digital image correlation (DIC) on a field of view of 5.5 x 4.1 mm(2) at the resolution of 2 mu m.pixel(-1), at a temperature of 22 degrees C and between 98 and 33% of relative humidity. At the end of the hydric loading, at dry state, the microstructure of the same field of view was mapped by an extended mosaic of scanning electron microscopy images at the resolution of 0.625 mu m.pixel(-1) and superimposed to the reference images used for DIC. Two microstructural parameters: the mean area and the area fraction of rigid clasts and clay matrix, were quantified by image analysis to be directly superimposed to local strain values. Speckle artefacts partly due to polished surfaces of clasts were filtered in the comparison between strains and microstructure. Strains concentrated in parts of the clay matrix, and at the interface between matrix and several quartz clasts which showed a slight detachment from the matrix. Constant clay and clast area fractions and sizes corresponded to very variable strain values at the microstructure scale. The relationship between strain values, mineral size and area fractions was not linear. Micro-mechanisms of deformation were therefore very complex at the scale of the experiment. On a very large field of view, very different microstructure behaviors were averaged which avoided any simple relationship between microstructure and strains. Heterogeneous water distribution and non-local microstructural control factors were suspected.
机译:本文提出了一种能够定量比较粘土材料的应变和微观结构的新方法。该方法适用于在实验室条件下承受循环液压载荷的Tournemire粘土岩样品。厘米大小的Tournemire粘土岩样品的局部应变通过数字图像相关(DIC)在5.5 x 4.1 mm(2)的视场上以2μm.pixel(-1)的分辨率在温度下进行定量温度为22摄氏度,相对湿度为98%至33%。在水压加载结束时,在干燥状态下,同一视野的微观结构通过扫描电子显微镜图像的扩展镶嵌图绘制,分辨率为0.625μm.pixel(-1),并叠加到参考图像上用于DIC。通过图像分析量化了两个参数:刚性碎屑和粘土基质的平均面积和面积分数,以直接叠加到局部应变值上。在应变和微观结构的比较中,部分滤除了碎屑表面的斑点伪影被过滤掉了。菌株集中在粘土基质的部分中,并且在基质与几个石英碎屑之间的界面处集中,该石英碎屑显示出与基质的轻微分离。恒定的粘土和碎屑面积分数和大小对应于在微结构尺度上非常变化的应变值。应变值,矿物大小和面积分数之间的关系不是线性的。因此,在实验规模上,变形的微观机制非常复杂。在很大的视野中,对平均非常不同的微观结构行为进行了平均,从而避免了微观结构与应变之间的任何简单关系。怀疑水分布不均和非局部的微观结构控制因素。

著录项

  • 来源
    《Applied clay science》 |2019年第12期|105244.1-105244.11|共11页
  • 作者单位

    CNRS Inst Rech Genie Civil & Mecan GeM Cent Nantes UMR 6183 1 Rue Noe F-44300 Nantes France|Univ Poitiers CNRS UMR 7285 HydrASA ENSI Poitiers IC2MP Bat B27 TSA 51106 4 Rue Michel Brunet F-86073 Poitiers 9 France;

    Univ Poitiers CNRS UMR 7285 HydrASA ENSI Poitiers IC2MP Bat B27 TSA 51106 4 Rue Michel Brunet F-86073 Poitiers 9 France;

    Univ Poitiers CNRS UPR 3346 Inst PPRIME SP 2 MI Bd M&P Curie Teleport 2 BP 30179 F-86962 Futuroscope France;

    Inst Radiol Protect & Nucl Safety DEI SARG Dept BP 17 F-92262 Fontenay Aux Roses France;

  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    Hydric loading; Strain; Tournemire clay rock; Microstructure; Phase area fraction; Digital image Correlation;

    机译:液压加载;应变;Tournemire粘土岩;微观结构相面积分数;数字图像相关;

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