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Evaluation of an ultrasonic extraction method compared with the Soxhlet extraction method for the determination of polyaromatic hydrocarbons and n-alkanes in airborne particulate matter

机译:评价超声提取法与索氏提取法相比,测定空气中颗粒物中的多环芳烃和正构烷烃

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摘要

An ultrasonic extraction method was evaluated for a GC/MS determination of polyaro- matic hydrocarbons (PAHs) and n-alkanes in airborne particulate matter, compared with the Soxhlet extraction method. Three airborne particulate samples collected at an industrial area of Kitakyushu City, a heavy traffic area of Kawasaki City, and Urban Dust (Standard Reference Material 1649) were extracted for seven PAHs and eight n-alkanes by both the ultrasonic extraction method with cyclohexane-ethanol (3 : 1) and Soxhlet extraction method with benzene-ethanol (3 : 1). Vehicle Exhaust Particulate (NIES No. 8) was also extracted for the compounds by the two methods. The results of the tar- get compounds by the ultrasonic extraction method well agreed with those by the Soxhlet extraction method, except for the vehicle exhaust particulate.
机译:与索氏提取法相比,评估了超声提取法对气载颗粒物质中的多环芳烃(PAHs)和正构烷烃进行GC / MS测定。在北九州市的工业区,川崎市的交通繁忙区和城市粉尘(标准参考材料1649)中采集的三个空气中悬浮颗粒样品通过环己烷-乙醇的超声提取方法分别提取了7种多环芳烃和8种正构烷烃。 (3∶1)和用苯乙醇(3∶1)的索氏提取法。还通过两种方法提取了汽车尾气颗粒(NIES No. 8)中的化合物。除汽车尾气中的颗粒物外,超声提取方法得到的目标化合物的结果与索氏提取方法得到的结果完全一致。

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