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A Clean-Green Synthesis of Platinum Nanoparticles Utilizing a Pernicious Weed Lantana (Lantana Camara)

机译:利用有害杂草马tana丹(马樱丹)清洁绿色合成铂纳米颗粒。

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摘要

A rapid, reproducible single step method is proposed for synthesizing platinum nanoparticles using an invasive weed lantana (Lantana camara, L). The method involves mixing of platinum (Ⅵ) solution, lantana leaf extract and ascorbic acid in appropriate concentrations and keeping the mixture at 95℃ for 8 min. The collective action of ascorbic acid and leaf extract reduced the chloroplatinic acid to platinum nanoparticles and leaf extract then served the additional purpose of stabilizing the nanoparticles. The resulting nanoparticles have an average size of 35 nm and crystallized in face centred cubic symmetry. The course of the synthesis was trekked by UV-visible spectrophotometry and the characterization of the nanoparticles was done with scanning electron microscopy and confocal laser Raman spectroscopy. Particle size distribution was estimated by dynamic light scattering and the crystal structure was determined by XRD. The purity of the product was checked by EDAX.
机译:提出了一种快速,可重复的单步方法,该方法用于使用入侵性杂草马tana丹(Lantana camara,L)合成铂纳米粒子。该方法包括将适当浓度的铂(Ⅵ)溶液,马樱丹叶提取物和抗坏血酸混合,并将混合物在95℃下保持8分钟。抗坏血酸和叶提取物的集体作用将氯铂酸还原为铂纳米颗粒,然后叶提取物具有稳定纳米颗粒的其他目的。所得纳米粒子的平均尺寸为35 nm,并以面心立方对称性结晶。紫外可见分光光度法测定了合成过程,用扫描电子显微镜和共聚焦激光拉曼光谱对纳米颗粒进行了表征。通过动态光散射估计粒度分布,并通过XRD确定晶体结构。产物的纯度通过EDAX检查。

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