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High Temperature Oxidation of Spark Plasma Sintered and Thermally Sprayed FeAl-Based Iron Aluminides

机译:火花等离子体烧结和热喷涂FeAl基铁铝化物的高温氧化

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摘要

The presented work deals with the oxidation resistance of spark plasma sintered and thermally sprayed FeAl-based intermetallics. Gas-atomized binary single phase Fe-43(at.%)Al and dual phase Fe-55(at.%)Al powders were used for spark plasma sintering and/or thermal spraying. Coatings were deposited by two different plasma spray technologies - gas and water stabilized plasma guns. The prepared samples were exposed to oxidation in artificial air at 700 ℃. The mass gain was measured during oxidation at 700 ℃ up to 1000 h. Microstructures, phase and chemical compositions of the formed scales were characterized after the exposition by means of scanning electron microscopy, X-ray diffraction and electron spectroscopy for chemical analysis (X-ray photoelectron spectroscopy).
机译:提出的工作涉及火花等离子体烧结和热喷涂FeAl基金属间化合物的抗氧化性。气雾化二元单相Fe-43(at。%)Al和双相Fe-55(at。%)Al粉末用于火花等离子体烧结和/或热喷涂。涂层是通过两种不同的等离子喷涂技术沉积的-气体和水稳定的等离子喷枪。制备的样品在700℃的人造空气中暴露于氧化。在700℃至1000 h的氧化过程中测定了质量增益。暴露后,通过扫描电子显微镜,X射线衍射和用于电子分析的电子光谱(X射线光电子能谱)对形成的氧化皮的微观结构,相和化学成分进行了表征。

著录项

  • 来源
    《Acta Physica Polonica》 |2012年第3期|465-468|共4页
  • 作者单位

    Czech Technical University in Prague, Faculty of Nuclear Sciences and Physical Engineering Department of Materials, Trojanova 13, 120 00 Prague 2, Czech Republic;

    Czech Technical University in Prague, Faculty of Nuclear Sciences and Physical Engineering Department of Materials, Trojanova 13, 120 00 Prague 2, Czech Republic;

    Research Centre Rez Ltd., Husinec-Rez 130, 250 68 Rez, Czech Republic;

    Institute of Chemical Technology Prague, Technicka 5, 166 28 Prague 6, Czech Republic;

    Institute of Plasma Physics AS CR, v. v. i., Department of Materials Engineering Za Slovankou 3, 182 00 Prague 8, Czech Republic;

    Max-Planck-Institut fuer Eisenforschung GmbH, Max-Planck-Str. 1, D-40237 Duesseldorf, Germany;

  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    metals, semimetals, and alloys; oxidation; powder processing: powder metallurgy, compaction, sintering, mechanical alloying, and granulation; spray coating techniques;

    机译:金属;半金属和合金;氧化粉末加工:粉末冶金;压实;烧结;机械合金化和造粒;喷涂技术;

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