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Flow injection analysis of nitrogen dioxide using a galvanic detector

机译:使用电流检测器对二氧化氮进行流动注射分析

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摘要

A flow injection configuration (FIA) based on a galvanic detector for the determination of nitrogen dioxide is described. The gaseous sample is directly injected into a gaseous carrier. The sample is transported toward the detector. The steady state measurements are not required to obtain the reproducible peak signals. The features of FIA are compared with that of continuous flow monitoring application. The flow injection system is simple, rapid and capable of detecting NO2 in the range of 1-500ppm (v/v). The measuring range and sensitivity of the galvanic detector in FIA depend on the sample volume. A relative standard deviation is 2.4% (n = 10) for 200ppm (v/v) of nitrogen dioxide. The sampling frequency is about 24 h-1
机译:描述了基于电流检测器的流动注入配置(FIA),用于确定二氧化氮。气态样品被直接注入气态载体中。样品被运送到检测器。不需要稳态测量即可获得可再现的峰值信号。将FIA的功能与连续流量监控应用程序的功能进行了比较。流动注射系统简单,快速,能够检测1-500ppm(v / v)范围内的NO2。 FIA中电流检测器的测量范围和灵敏度取决于样品量。对于200ppm(v / v)的二氧化氮,相对标准偏差为2.4%(n = 10)。采样频率约为24 h -1

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