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Fabrication and Characterization of Gelatin Stabilized Silver Nanoparticles under UV-Light

机译:紫外光下明胶稳定的银纳米粒子的制备与表征

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摘要

Silver nanoparticles (Ag-NPs) were successfully synthesized using the UV irradiation of aqueous solutions containing AgNO3 and gelatin as a silver source and stabilizer, respectively. The UV irradiation times influence the particles’ diameter of the Ag-NPs, as evidenced from surface plasmon resonance (SPR) bands and transmission electron microscopy (TEM) images. When the UV irradiation time was increased, the mean size of particles continuously decreased as a result of photoinduced Ag-NPs fragmentation. Based on X-ray diffraction (XRD), the UV-irradiated Ag-NPs were a face-centered cubic (fcc) single crystal without any impurity. This study reveals that the UV irradiation-mediated method is a green chemistry and promising route for the synthesis of stable Ag-NPs for several applications (e.g., medical and surgical devices). The important advantages of this method are that it is cheap, easy, and free of toxic materials.
机译:分别使用含有AgNO3和明胶作为银源和稳定剂的水溶液进行紫外线照射,成功地合成了银纳米颗粒(Ag-NPs)。从表面等离子体共振(SPR)谱带和透射电子显微镜(TEM)图像可以证明,紫外线照射时间会影响Ag-NP的粒径。当增加紫外线照射时间时,由于光诱导的Ag-NPs碎裂,颗粒的平均尺寸连续减小。基于X射线衍射(XRD),紫外线照射的Ag-NPs是面心立方(fcc)单晶,没有任何杂质。这项研究表明,紫外线辐射介导的方法是绿色化学,是用于多种应用(例如医疗和外科手术设备)的稳定Ag-NP合成的有前途的途径。这种方法的重要优点是便宜,容易并且没有有毒物质。

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