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One-step green synthesis and characterization of leaf extract-mediated biocompatible silver and gold nanoparticles from Memecylon umbellatum

机译:叶提取物介导的Memecylon umbellatum的生物相容性银和金纳米粒子的一步绿色合成和表征

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摘要

In this experiment, green-synthesized silver and gold nanoparticles were produced rapidly by treating silver and gold ions with an extract of Memecylon umbellatum leaf. The reaction process was simple and easy to handle, and was monitored using ultraviolet-visible spectroscopy. The effect of the phytochemicals present in M. umbellatum, including saponins, phenolic compounds, phytosterols, and quinones, on formation of stable silver and gold nanoparticles was investigated by Fourier-transform infrared spectroscopy. The morphology and crystalline phase of the nanoparticles were determined by transmission electron microscopy and energy-dispersive x-ray spectroscopy. The results indicate that the saponins, phytosterols, and phenolic compounds present in the plant extract play a major role in formation of silver and gold nanoparticles in their respective ions in solution. The characteristics of the nanoparticles formed suggest application of silver and gold nanoparticles as chemical sensors in the future. Given the simple and eco-friendly approach for synthesis, these nanoparticles could easily be commercialized for large-scale production.
机译:在该实验中,通过用伞形Memecylon umbellatum叶提取物处理银和金离子,可以快速生产出绿色合成的银和金纳米颗粒。该反应过程简单且易于处理,并使用紫外-可见光谱进行监测。通过傅立叶变换红外光谱法研究了伞形藻中存在的植物化学物质,包括皂苷,酚类化合物,植物甾醇和醌,对形成稳定的银和金纳米颗粒的影响。纳米颗粒的形态和结晶相通过透射电子显微镜和能量色散X射线光谱法测定。结果表明,植物提取物中存在的皂甙,植物甾醇和酚类化合物在溶液中各自离子中的银和金纳米颗粒的形成中起主要作用。形成的纳米颗粒的特性表明,将来将银和金的纳米颗粒用作化学传感器。考虑到简单且环保的合成方法,这些纳米粒子可以很容易地商业化用于大规模生产。

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