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Absolute Configuration Determination of Retroflexanone Using the Advanced Mosher Method and Application of HPLC-NMR

机译：先进的莫舍尔法测定逆苯呋喃酮的绝对构型及HPLC-NMR的应用

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摘要

The absolute configuration of retroflexanone (>1) and a closely related phlorogluinol (>2) was established using the advanced Mosher method and by application of HPLC-NMR. HPLC-NMR permitted a small scale Mosher method analysis to be carried out on these unstable phloroglucinols.

机译：使用先进的Mosher方法并通过HPLC-NMR建立了逆反射酮（> 1 ）和密切相关的间苯三酚（> 2 ）的绝对构型。 HPLC-NMR允许对这些不稳定的间苯三酚进行小规模的Mosher方法分析。

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期刊名称 Marine Drugs
作者
Caleb Singleton; Robert Brkljača; Sylvia Urban;
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作者单位

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年(卷),期 2018(16),6
年度 2018
页码 205
总页数 9
原文格式 PDF
正文语种
中图分类药物化学;
关键词
Mosher retroflexanone phloroglucinol HPLC-NMR secondary alcohol;

机译：催乳剂;逆苯醌;间苯三酚;HPLC-NMR;仲醇;

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专利

1. Absolute Configuration Determination of Retroflexanone Using the Advanced Mosher Method and Application of HPLC-NMR [J] . Caleb Singleton, Robert Brklja?a, Sylvia Urban Marine Drugs . 2018,第6期

机译：先进莫舍尔法测定逆转录福酮的绝对构型及HPLC-NMR的应用
2. Application of a modified Mosher's method for the determination of enantiomeric ratio and absolute configuration at C-3 of chiral 1,3-dihydroxy ketones [J] . Galman JL, Hailes HC Tetrahedron, Asymmetry: The International Journal for Repid Publication on all Aspects of Asymmetry in Orgainc, Inorganic, Organometallic, Physical and Bio-Organic Chemistry . 2009,第15期

机译：改进的Mosher方法在测定手性1,3-二羟基酮的C-3对映体比率和绝对构型中的应用
3. Determination of absolute configuration of photo-degraded catechinopyranocyanidin A by modified Mosher's method [J] . Oyama Kin-ichi, Kondo Tadao, Shimizu Toshimichi, Chirality: The pharmacological, biological, and chemical consequences of molecular asymmetry . 2020,第5期

机译：改性Mosher方法测定光降解的摄影药物嘧啶霉素A的绝对结构
4. Absolute Configuration Determination by ECD, 1HNMR,and X-Ray Methods: Principles Applications [C] . Nobuyuki Harada The 5th symposium on molecular chirality of Chinese Chemical Society amp; International Chiral Meeting . 2012

机译：通过ECD，1HNMR和X射线方法确定绝对构型：原理与应用
5. Determination of the Absolute Configuration of β-Chiral Primary Alcohols Using the Competing Enantioselective Conversion Method Heteroatom-directed Acylation of Secondary Alcohols to Assign Absolute Configuration Total Synthesis of Illisimonin a Osmate Es [D] . Burns, Alexander Sunshine. 2020

机译：使用竞争对映选择性转化法测定β-chiral初级醇的绝对构型次原子为仲醇的酰化酰化，分配绝对构型Illisimonin的总合成渗透
6. Total Synthesis of Gobiusxanthin Stereoisomers and Their Application to Determination of Absolute Configurations of Natural Products: Revision of Reported Absolute Configuration of Epigobiusxanthin [O] . Yumiko Yamano, Kotaro Ematsu, Hiromasa Kurimoto, 2015

机译：高比色黄质立体异构体的全合成及其在确定天然产物的绝对构型中的应用：对表必高黄嘌呤的报道的绝对构型的修订
7. Absolute Configuration Determination of Retroflexanone Using the Advanced Mosher Method and Application of HPLC-NMR [O] . Caleb Singleton, Robert Brkljača, Sylvia Urban 2018

机译：使用先进的MOSHER方法和HPLC-NMR的应用来确定逆框隆的绝对配置确定
8. Determination of wind tunnel constraint effects by a unified pressure signature method. Part 1: Applications to winged configurations [R] . Hackett, J. E., Sampath, S., Phillips, C. G. 1981

机译：用统一压力特征法确定风洞约束效应。第1部分：有翼配置的应用

Absolute Configuration Determination of Retroflexanone Using the Advanced Mosher Method and Application of HPLC-NMR

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