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High-Speed Fabrication of Clear Transparent Cellulose Nanopaper by Applying Humidity-Controlled Multi-Stage Drying Method

机译:涂布湿度控制的多阶段干燥方法清除透明纤维素纳米锅的高速制备

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摘要

As a renewable nanomaterial, transparent nanopaper is one of the promising materials for electronic devices. Although conventional evaporation drying method endows nanopaper with superior optical properties, the long fabrication time limits its widely use. In this work, we propose a multi-stage drying method to achieve high-speed fabrication of clear transparent nanopaper. Drying experiments reveal that nanopaper’s drying process can be separated into two periods. For the conventional single-stage evaporation drying, the drying condition is kept the same. In our newly proposed multi-stage drying, the relative humidity (RH), which is the key parameter for both drying time and haze, is set differently during these two periods. Applying this method in a humidity-controllable environmental chamber, the drying time can be shortened by 35% (from 11.7 h to 7.6 h) while maintaining the same haze level as that from single-stage drying. For a conventional humidity-uncontrollable oven, a special air flow system is added. The air flow system enables decrease of RH by removing water vapor at the water/air interface during the earlier period, thus fabricating clear transparent nanopaper in a relatively short time. Therefore, this humidity-controlled multi-stage drying method will help reduce the manufacturing time and encourage the widespread use of future nanopaper-based flexible electronics.
机译:作为可再生纳米材料,透明纳米纸是电子设备的有希望的材料之一。尽管常规蒸发干燥方法赋予具有优异光学性质的纳米锅,但长度的制造时间限制了其广泛使用。在这项工作中,我们提出了一种多级干燥方法,实现清晰透明纳米锅的高速制造。干燥实验表明,纳米锅的干燥过程可以分为两个时期。对于传统的单级蒸发干燥,干燥条件保持相同。在我们新提出的多级干燥中,在这两个时段期间,相对湿度(RH)是用于干燥时间和雾度的关键参数。将该方法在湿度可控的环境室中应用,干燥时间可以缩短35%(从11.7小时至7.6小时),同时保持与单级干燥相同的雾度水平。对于传统的湿度无法控制的烤箱,添加了一种特殊的空气流量系统。气流系统通过在早期的时间内去除水/空气接口处的水蒸气来降低RH,从而在相对较短的时间内制造清晰的透明纳米件。因此,这种湿度控制的多级干燥方法将有助于降低制造时间,并鼓励广泛使用未来的基于纳米纸针的柔性电子。

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