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The Potential of Pandanus amaryllifolius Leaves Extract in Fabrication of Dense and Uniform ZnO Microrods

机译:露兜树叶片提取物在致密均匀的ZnO微棒制备中的潜力

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摘要

Zinc oxide (ZnO) micro and nanorods were successfully prepared using and hexamethylenetetramine (HMTA) separately as stabilizers using the solution immersion method. Two types of ZnO seed layer were prepared using the same pre-cursor with the different stabilizers. The fabricated ZnO microrods exhibit absorption at ~375 nm as revealed from the UV–Visible absorption spectrum, and this is comparable with ZnO nanorods synthesized using HMTA. X-ray diffraction (XRD) measurement displayed a sharp peak corresponding to the hexagonal wurtzite structure of ZnO microrods. Field emission scanning electron microscopy (FESEM) of ZnO microrods showed average diameter at approximately 500 nm compared to 70 nm of those synthesized from HMTA. A new finding is the ability of as a green stabilizer to grow a dense ZnO microrod structure with high crystallinity. Results reveal that both samples from different stabilizers during the preparation of the ZnO seed layer greatly improved the morphological and structural properties and optical absorption of ZnO. The main outcomes from this study will benefit optoelectronic application, such as in ultraviolet (UV) sensors.
机译:分别采用六亚甲基四胺(HMTA)和六亚甲基四胺(HMTA)作为稳定剂,采用溶液浸渍法成功制备了氧化锌(ZnO)微纳米棒。使用相同的前体和不同的稳定剂制备了两种类型的ZnO晶种层。从紫外可见吸收光谱可知,所制备的ZnO微棒在〜375 nm处表现出吸收,这与使用HMTA合成的ZnO纳米棒相当。 X射线衍射(XRD)测量显示了一个尖峰,该峰对应于ZnO微棒的六角纤锌矿结构。 ZnO微棒的场发射扫描电子显微镜(FESEM)显示平均直径约为500 nm,而从HMTA合成的平均直径为70 nm。一个新发现是作为绿色稳定剂能够生长具有高结晶度的致密ZnO微棒结构的能力。结果表明,在制备ZnO晶种层时,来自不同稳定剂的两个样品均极大地改善了ZnO的形态,结构性能和光吸收性。这项研究的主要成果将有益于光电应用,例如在紫外线(UV)传感器中的应用。

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