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Preparation Characteristics and Application of Bifunctional TiO2 Sheets

机译:双功能TiO2片材的制备特性及应用

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摘要

TiO is a high-reflectance material for preparing sheets during dry reagent chemical tests in detail. In this study, bifunctional TiO sheets with diffusive and reflective properties were prepared using TiO microspheres (particle size 2–3 µm) and cellulose acetate (CA). Factors such as the CA dosage, water content, mixing time, and the choice of surfactant were investigated. The structure and properties of the bifunctional TiO sheets were characterized by thermogravimetry and differential thermal analysis (TG-DAT), scanning electron microscopy (SEM), dynamic contact angle test and reflectance spectroscopy. By studying the above experimental results, it was concluded that the most optimal preparation conditions for preparing the bi-functional TiO sheets under natural drying conditions were as follows: the mass ratio of CA to TiO microspheres was 0.05:1; Triton-100 was used to improve the diffusion performance of the bifunctional sheets, after mixing for 5 h and coating. The light reflectivity of the bifunctional TiO sheets in the 420 to 800 nm range was higher than 90%. Serum diffused in the bifunctional TiO sheets reacted in the reagent sheets and formed uniform colorful spots. Considering the repeatability of spot proportion and light reflectivity, the sheet offered a uniform serum diffusion and good repeatability. So, the bifunctional TiO sheets are nominated as a promising material for dry chemical diagnostic reagents.
机译:TiO是一种高反射率的材料,用于在干试剂化学测试中详细制备薄片。在这项研究中,使用TiO微球(粒径2-3 µm)和醋酸纤维素(CA)制备了具有扩散和反射特性的双功能TiO片。研究了CA用量,水含量,混合时间和表面活性剂的选择等因素。通过热重分析和差热分析(​​TG-DAT),扫描电子显微镜(SEM),动态接触角测试和反射光谱对双功能TiO片材的结构和性能进行了表征。通过对上述实验结果的研究得出结论,在自然干燥条件下制备双功能TiO片的最佳制备条件为:CA与TiO微球的质量比为0.05:1;混合5小时并涂覆后,使用Triton-100改善双功能片的扩散性能。在420至800nm范围内的双功能TiO片的光反射率高于90%。分散在双功能TiO片中的血清在试剂片中反应并形成均匀的彩色斑点。考虑到斑点比例和光反射率的可重复性,该薄片提供了均匀的血清扩散和良好的可重复性。因此,双功能TiO片被提名为干化学诊断试剂的有前途的材料。

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