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Data of preparation and characterization of activated carbon using two activant agents and mango seed as precursor material

机译:以两种活化剂和芒果籽为前驱体材料制备和表征活性炭的数据

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摘要

The aim of this research is to prepare various carbonaceous materials with different textural, structural and chemical characteristics, using mango seed a rarely used residue for the preparation of activated carbons, as the precursor material. The mango seed was analyzed by TGA and SEM also methodological data about the preparation of activated carbons are provided. Four activated carbons were prepared using sulfuric acid (H SO ) and calcium chloride (CaCl ) as activating agents and were characterized by means of TGA, SEM/EDX, Boehm Titration, isotherm determination of N adsorption-desorption at −196 °C and immersion calorimetry. Four carbons were obtained with superficial areas BET between 6 and 33 m  g and different chemical characteristics associated with the changes in the concentration of the activating agents. The activated carbons that were prepared with the highest activating agent concentrations, obtained better results in the amount of oxygenated surface groups, the total acidity and the amount of fixed carbon. The enthalpy of immersion in water was between 7 and 16 J g .
机译:这项研究的目的是使用芒果籽(一种很少使用的残留物来制备活性炭)作为前体材料,以制备具有不同结构,结构和化学特性的各种含碳材料。通过TGA和SEM对芒果种子进行了分析,并提供了有关活性炭制备的方法学数据。使用硫酸(H SO)和氯化钙(CaCl)作为活化剂制备了四种活性炭,并通过TGA,SEM / EDX,Boehm滴定,在-196°C下等温测定N的吸附-脱附和浸没进行了表征量热法。获得了四个碳,其表面积BET在6到33 mg之间,并且化学性质与活化剂浓度的变化有关。用最高活化剂浓度制备的活性炭在含氧表面基团的量,总酸度和固定碳的量方面获得了更好的结果。浸入水中的焓为7至16 Jg。

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