A sulfane sulfur mediated benzodithiolone formation was developed. Based on this reaction, two fluorescent probes (>SSP1 and >SSP2) for the detection of sulfane sulfur species (persulfide, polysulfide, and elemental sulfur) were prepared and evaluated. The probes showed high selectivity and sensitivity to sulfane sulfurs. Moreover, >SSP2 was successfully applied for bioimaging sulfane sulfurs in living cells.
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