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Surface Characteristics and Bioactivity of a Novel Natural HA/Zircon Nanocomposite Coated on Dental Implants

机译:新型天然HA /锆石纳米复合材料在牙种植体上的表面特性和生物活性

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摘要

The surface characteristics of implant which influence the speed and strength of osseointegration include surface chemistry, crystal structure and crystallinity, roughness, strain hardening, and presence of impurities. The aim of this study was to evaluate the bioactivity and roughness of a novel natural hydroxyapatite/zircon (NHA/zircon) nanobiocomposite, coated on 316L stainless steel (SS) soaked in simulated body fluid (SBF). NHA/zircon nanobiocomposite was fabricated with 0 wt.%, 5 wt.%, 10 wt.%, and 15 wt.% of zircon in NHA using ball mill for 20 minutes. The composite mixture was coated on 316L SS using plasma spray method. The results are estimated using the scanning electron microscopy (SEM) observation to evaluate surface morphology, X-ray diffraction (XRD) to analyze phase composition, and transmission electron microscopy (TEM) technique to evaluate the shape and size of prepared NHA. Surfaces roughness tester was performed to characterize the coated nanocomposite samples. The maximum average R a (14.54 μm) was found in the NHA 10 wt.% of zircon coating. In addition, crystallinity (X c) was measured by XRD data, which indicated the minimum value (X c = 41.1%) for the sample containing 10 wt.% of zircon. Maximum bioactivity occurred in the sample containing 10 wt.% of zircon, which was due to two reasons: first, the maximum roughness and, second, the minimum crystallinity of nanobiocomposite coating.
机译:影响骨整合速度和强度的植入物表面特征包括表面化学性质,晶体结构和结晶度,粗糙度,应变硬化和杂质的存在。这项研究的目的是评估一种新型的天然羟基磷灰石/锆石(NHA /锆石)纳米生物复合材料的生物活性和粗糙度,该复合材料涂覆在浸入模拟体液(SBF)中的316L不锈钢(SS)上。使用球磨机,用NHA中0%(重量),5%(重量),10%(重量)和15%(重量)的锆石制造NHA /锆石纳米生物复合材料。使用等离子喷涂方法将复合混合物涂覆在316L SS上。使用扫描电子显微镜(SEM)观察以评估表面形态,使用X射线衍射(XRD)分析相组成以及使用透射电子显微镜(TEM)技术评估所制备的NHA的形状和尺寸来估算结果。进行表面粗糙度测试仪以表征涂覆的纳米复合材料样品。在NHA 10%(重量)的锆石涂层中发现了最大平均Ra(14.54μm)。另外,通过XRD数据测量结晶度(X c),该结晶度(X c)指示含有10重量%的锆石的样品的最小值(X c == 41.1%)。在含有10%(重量)的锆石的样品中发生了最大的生物活性,这是由于两个原因:第一,纳米生物复合涂层的最大粗糙度,第二,最小的结晶度。

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