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Assay reproducibility of serum androgen measurements using liquid chromatography-tandem mass spectrometry

机译：液相色谱-串联质谱法测定血清雄激素的测定重现性

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摘要

BackgroundValid and precise measures of androgen concentrations are needed for etiologic studies of hormonally-related cancers. We developed a high-performance liquid chromatography-tandem mass spectrometry (LC-MS/MS) method with two sample preparations to measure 11 androgens, including adrenal and gonadal androgenic precursors and their 5α-reduced metabolites.

机译：背景技术对于激素相关癌症的病因研究，需要有效和精确的雄激素浓度测量。我们开发了一种高效液相色谱-串联质谱（LC-MS / MS）方法，其中有两种样品制备方法可测量11种雄激素，包括肾上腺和性腺雄激素前体及其5α还原代谢产物。

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期刊名称 other
作者
Britton Trabert; Xia Xu; Roni T. Falk; Chantal Guillemette; Frank Z. Stanczyk; Katherine A. McGlynn;
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作者单位

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年(卷),期 -1(155),0 0
年度 -1
页码 56–62
总页数 16
原文格式 PDF
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关键词
reproducibility serum androgen assay liquid chromatography tandem mass spectrometry metabolites endogenous hormones;

机译：重现性;血清雄激素测定;液相色谱串联质谱;代谢产物;内源激素;

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专利

1. Assay reproducibility of serum androgen measurements using liquid chromatography-tandem mass spectrometry [J] . Trabert Britton, Xu Xia, Falk Roni T., The Journal of Steroid Biochemistry and Molecular Biology . 2016,第Pta1期

机译：液相色谱-串联质谱法测定血清雄激素的测定重现性
2. Development and validation of a sensitive liquid chromatography-tandem mass spectrometry assay to simultaneously measure androgens and estrogens in serum without derivatization. [J] . Harwood DT, Handelsman DJ Clinica chimica acta: International journal of clinical chemistry and applied molecular biology . 2009,第1a2期

机译：灵敏液相色谱-串联质谱分析法的开发和验证，该方法可同时测量血清中的雄激素和雌激素而无需衍生化。
3. Simultaneous measurement of amiodarone and desethylamiodarone in human plasma and serum by stable isotope dilution liquid chromatography-tandem mass spectrometry assay. [J] . Kuhn J, Gotting C, Kleesiek K Journal of Pharmaceutical and Biomedical Analysis: An International Journal on All Drug-Related Topics in Pharmaceutical, Biomedical and Clinical Analysis . 2010,第1期

机译：稳定同位素稀释液相色谱-串联质谱法同时测定人血浆和血清中的胺碘酮和去乙基胺碘酮。
4. Stable-Isotope Dilution Liquid Chromatography-Tandem Mass Spectrometry Assay for the Quantification of Testosterone in Human Plasma for Use in the Clinical Diagnosis of Androgen-Mediated Diseases [C] . Xueheng Zhao, Kenneth D.R. Setchell ASMS Conference on Mass Spectrometry and Allied Topics . 2008

机译：稳定同位素稀释液相色谱 - 串联质谱法测定人血浆中睾酮中的睾酮，用于癌症介导的雌激素介导的疾病的临床诊断
5. Characterization of Clandestine One Pot Methamphetamine Laboratories Using Gas Chromatography-Mass Spectrometry and Liquid Chromatography-Tandem Mass Spectrometry [D] . Ciesielski, Austin Lee. 2017

机译：气相色谱-质谱联用和液相色谱-串联质谱联用对秘密的一锅甲基苯丙胺实验室进行表征
6. Reproducibility of an assay to measure serum progesterone metabolites that may be related to breast cancer risk using liquid chromatography-tandem mass spectrometry [O] . Britton Trabert, Roni T. Falk, Frank Z. Stanczyk, -1

机译：使用液相色谱-串联质谱法测定可能与乳腺癌风险相关的血清孕酮代谢物的测定法的可重复性
7. Assay reproducibility of serum androgen measurements using liquid chromatography–tandem mass spectrometry [O] . Britton Trabert, Xia Xu, Roni T. Falk, 2016

机译：使用液相色谱 - 串联质谱法测定血清雄激素测量的再现性

Assay reproducibility of serum androgen measurements using liquid chromatography-tandem mass spectrometry

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