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Nanoscale elastic modulus of single horizontal ZnO nanorod using nanoindentation experiment

机译:纳米压痕实验研究单水平ZnO纳米棒的纳米尺度弹性模量

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摘要

We measure the elastic modulus of a single horizontal ZnO nanorod [NR] grown by a low-temperature hydrothermal chemical process on silicon substrates by performing room-temperature, direct load-controlled nanoindentation measurements. The configuration of the experiment for the single ZnO NR was achieved using a focused ion beam/scanning electron microscope dual-beam instrument. The single ZnO NR was positioned horizontally over a hole on a silicon wafer using a nanomanipulator, and both ends were bonded with platinum, defining a three-point bending configuration. The elastic modulus of the ZnO NR, extracted from the unloading curve using the well-known Oliver-Pharr method, resulted in a value of approximately 800 GPa. Also, we discuss the NR creep mechanism observed under indentation. The mechanical behavior reported in this paper will be a useful reference for the design and applications of future nanodevices.
机译:我们通过执行室温,直接负载控制的纳米压痕测量,来测量通过低温水热化学工艺在硅基板上生长的单个水平ZnO纳米棒[NR]的弹性模量。使用聚焦离子束/扫描电子显微镜双束仪器实现了单ZnO NR的实验配置。使用纳米操纵器将单个ZnO NR水平放置在硅晶片上的孔上,两端用铂键合,形成三点弯曲结构。使用众所周知的Oliver-Pharr方法从卸荷曲线中提取的ZnO NR的弹性模量约为800 GPa。此外,我们讨论了在压痕下观察到的NR蠕变机理。本文报道的机械性能将为未来纳米器件的设计和应用提供有用的参考。

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