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Rotatable precipitates change the scale-free to scale dependent statistics in compressed Ti nano-pillars

机译:可旋转的沉淀物改变了压缩Ti纳米柱的无标度到标度的统计

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摘要

Compressed nano-pillars crackle from moving dislocations, which reduces plastic stability. Crackling noise is characterized by stress drops or strain bursts, which scale over a large region of sizes leading to power law statistics. Here we report that this “classic” behaviour is not valid in Ti-based nanopillars for a counterintuitive reason: we tailor precipitates inside the nano-pillar, which “regulate” the flux of dislocations. It is not because the nano-pillars become too small to sustain large dislocation movements, the effect is hence independent of size. Our precipitates act as “rotors”: local stress initiates the rotation of inclusions, which reduces the stress amplitudes dramatically. The size distribution of stress drops simultaneously changes from power law to exponential. Rotors act like revolving doors limiting the number of passing dislocations. Hence each collapse becomes weak. We present experimental evidence for Ti-based nano-pillars (diameters between 300 nm and 2 μm) with power law distributions of crackling noise P(s) ∼ s−τ with τ ∼ 2 in the defect free or non-rotatable precipitate states. Rotors change the size distribution to P(s) ∼ exp(−s/s0). Rotors are inclusions of ω-phase that aligns under stress along slip planes and limit dislocation glide to small distances with high nucleation rates. This opens new ways to make nano-pillars more stable.
机译:压缩的纳米柱因位错移动而破裂,从而降低了塑料的稳定性。爆裂噪声的特征在于应力降或应变突发,应力降或应变突发在较大的尺寸区域内缩放,从而导致幂律统计。在这里,我们报告说,出于直觉的原因,这种“经典”行为在Ti基纳米柱中无效:我们在纳米柱内部定制了沉淀物,这些沉淀物“调节”了位错的通量。这不是因为纳米柱变得太小而无法承受较大的位错运动,因此效果与尺寸无关。我们的沉淀物起“转子”的作用:局部应力引发夹杂物的旋转,从而极大地降低了应力振幅。应力降的大小分布同时从幂律变为指数。转子就像旋转门一样,限制了通过位错的数量。因此,每次崩溃都变得微弱。我们提供了Ti基纳米柱(直径在300 nm至2μm之间)的实验证据,该裂纹的裂隙噪声P(s)〜s 的幂律分布为τ〜2,且无缺陷或不可旋转的沉淀状态。转子将尺寸分布更改为P(s)〜exp(-s / s0)。转子是ω相的夹杂物,它们在应力作用下沿着滑移面对齐,并以高成核率将位错滑移限制到较小的距离。这开辟了使纳米柱更稳定的新方法。

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