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Quantitative Metallography With a Digital Computer: Application to a Nb-Sn Superconducting Wire

机译:数字计算机定量金相学:在Nb-Sn超导线材中的应用

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摘要

Accurate quantitative data pertinent to the structure of solid materials at the micro size level, which are difficult or prohibitive to obtain by traditional manual measurements, are now obtained directly by a digital computer which uses a photomicrograph as the information input. The history of picture interpretation experiments at the National Bureau of Standards is reviewed. The fundamental computer operations are illustrated, together with a description of 24 image processing routines now functional at a practical level.A micrograph of a specimen of Nb-Sn superconductor wire is exhaustively analyzed. This specimen is found to contain approximately 70 percent Nb3Sn, nearly all of which is mutually interconnected. It is also found that in this specimen the mean free path in the Nb3Sn superconducting phase is only 26.5 microns. This small value results from the spongy structure of the material and numerous interruptions caused by voids and by particles of four other solid phases. The comparative importance of the several types of interruptions is measured. It is determined that small voids are the most important single cause of the short mean free path, and deduced that these voids appear to have formed mainly from the reaction during heat treatment.
机译:现在,通过使用显微照片作为信息输入的数字计算机可以直接获得与固体材料结构有关的精确定量数据,而这些数据很难或无法通过传统的手动测量获得,因此可以在微米级水平上进行测量。回顾了国家标准局的图片解释实验的历史。举例说明了计算机的基本操作,并描述了现已实用的24种图像处理程序。详尽地分析了Nb-Sn超导体样品的显微照片。发现该样品含有大约70%的Nb3Sn,几乎所有的Nb3Sn都是相互连接的。还发现在该样品中,Nb3Sn超导相的平均自由程仅为26.5微米。该较小的值是由于材料的海绵状结构以及由空隙和其他四个固相的颗粒引起的大量中断所致。测量了几种类型的中断的相对重要性。已确定小空隙是平均自由程短的最重要的单一原因,并推断出这些空隙似乎主要是由热处理过程中的反应形成的。

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